(R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoic acid

Base Information

Chemical Name:(R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoic acid
CAS No.:942999-01-1
Molecular Formula:C₁₇H₂₅NO₅
Molecular Weight:323.389
Hs Code.:

Synonyms:(R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoic acid

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Chemical Property of (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoic acid

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Technology Process of (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoic acid

There total 5 articles about (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 942999-00-0
methyl (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoate

: 942999-01-1
(R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoic acid

Guidance literature:: methyl (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoate; With potassium hydroxide; In methanol; water; at 50 ℃; for 3h;

With hydrogenchloride; In water;

Reference yield:

: 352705-03-4
(2R)-2-[(tert-butoxycarbonyl)amino]propyl 4-methylbenzene-1-sulfonate

: 942999-01-1
(R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: CsCO₃ / N,N-dimethyl-formamide / 50 °C

2: potassium hydroxide / methanol / 3 h / 50 °C

With potassium hydroxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm701359z

Reference yield:

: 4919-37-3
3,5-dimethyl-4-hydroxybenzoic acid

: 942999-01-1
(R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / 3 h / Heating

2: CsCO₃ / N,N-dimethyl-formamide / 50 °C

3: potassium hydroxide / methanol / 3 h / 50 °C

With hydrogenchloride; potassium hydroxide; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm701359z