methyl (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoate

Base Information

Chemical Name:methyl (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoate
CAS No.:942999-00-0
Molecular Formula:C₁₈H₂₇NO₅
Molecular Weight:337.416
Hs Code.:

Synonyms:methyl (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoate

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Technology Process of methyl (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoate

There total 3 articles about methyl (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 352705-03-4
(2R)-2-[(tert-butoxycarbonyl)amino]propyl 4-methylbenzene-1-sulfonate

: 34137-14-9
methyl 4-hydroxy-3,5-dimethylbenzoate

: 942999-00-0
methyl (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoate

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 50 ℃;

Reference yield:

: 79069-13-9,127516-56-7,147252-84-4,106391-86-0
(R)-2-tertbutoxycarbonylamino-1-propanol

: 942999-00-0
methyl (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 0 - 20 °C

2: CsCO₃ / N,N-dimethyl-formamide / 50 °C

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1021/jm701359z

Reference yield:

: 4919-37-3
3,5-dimethyl-4-hydroxybenzoic acid

: 942999-00-0
methyl (R)-4-[2-(tert-butyloxycarbonylamino)propyloxy]-3,5-dimethylbenzoate

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 3 h / Heating

2: CsCO₃ / N,N-dimethyl-formamide / 50 °C

With hydrogenchloride; In N,N-dimethyl-formamide;
DOI:10.1021/jm701359z