5-acetyl-2-(3-azidopropoxy)benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester

Base Information

• Chemical Name: 5-acetyl-2-(3-azidopropoxy)benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester
• CAS No.: 946570-28-1
• Molecular Formula: C₁₆H₁₆N₄O₆
• Molecular Weight: 360.326

Synonyms:5-acetyl-2-(3-azidopropoxy)benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester

Chemical Property of 5-acetyl-2-(3-azidopropoxy)benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester

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Technology Process of 5-acetyl-2-(3-azidopropoxy)benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester

There total 2 articles about 5-acetyl-2-(3-azidopropoxy)benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-acetyl-2-(3-azidopropoxy)benzoic acid (946570-27-0) + O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate (105832-38-0) → 5-acetyl-2-(3-azidopropoxy)benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester (946570-28-1)

Guidance literature:

With triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 24h;

Reference yield:

sodium hydrogen sulfate (7681-38-1) + 5-acetyl-2-(3-azidopropoxy)benzoic acid (946570-27-0) + O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate (105832-38-0) → 5-acetyl-2-(3-azidopropoxy)benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester (946570-28-1)

Guidance literature:

With triethylamine; In n-heptane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

5-acetyl-2-(3-azidopropoxy)benzoic acid 2,5-dioxo-pyrrolidin-1-yl ester (946570-28-1) + [(S)-5-amino-1-carbamoylpentyl]carbamic acid tert-butyl ester (58725-24-9) → {(S)-5-[5-acetyl-2-(3-azidopropoxy)benzoylamino]-1-[carbamoyl]pentyl}carbamic acid tert-butyl ester (946570-30-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

upstream raw materials:

5-acetyl-2-(3-azidopropoxy)benzoic acid

O-(N-succinimidyl)-N,N,N',N'-tetramethyluronium tetrafluoroborate

sodium hydrogen sulfate

Downstream raw materials:

{(S)-5-[5-acetyl-2-(3-azidopropoxy)benzoylamino]-1-[carbamoyl]pentyl}carbamic acid tert-butyl ester

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