Technology Process of C27H26BrNO5
There total 4 articles about C27H26BrNO5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
acetic acid; tetramethylammonium triacetoxyborohydride;
In
acetonitrile;
at 20 ℃;
for 3h;
Inert atmosphere;
DOI:10.1021/jm101318b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanol; dichloromethane / 0 °C / Inert atmosphere; UV-irradiation
2: sodium methylate / methanol / 0 - 60 °C / Inert atmosphere
3: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 3 h / 20 °C / Inert atmosphere
With
sodium methylate; acetic acid; tetramethylammonium triacetoxyborohydride;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1021/jm101318b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanol; dichloromethane / 0 °C / Inert atmosphere; UV-irradiation
2: sodium methylate / methanol / 0 - 60 °C / Inert atmosphere
3: acetic acid; tetramethylammonium triacetoxyborohydride / acetonitrile / 3 h / 20 °C / Inert atmosphere
With
sodium methylate; acetic acid; tetramethylammonium triacetoxyborohydride;
In
methanol; dichloromethane; acetonitrile;
DOI:10.1021/jm101318b