(E)-6-(2-(3-oxazolidinyl)ethoxy)-2-(4-dimethylaminostyryl)benzofuran hydrochloride

Base Information

Chemical Name:(E)-6-(2-(3-oxazolidinyl)ethoxy)-2-(4-dimethylaminostyryl)benzofuran hydrochloride
CAS No.:1462470-08-1
Molecular Formula:C₂₃H₂₆N₂O₃*ClH
Molecular Weight:414.932
Hs Code.:

Synonyms:(E)-6-(2-(3-oxazolidinyl)ethoxy)-2-(4-dimethylaminostyryl)benzofuran hydrochloride

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Chemical Property of (E)-6-(2-(3-oxazolidinyl)ethoxy)-2-(4-dimethylaminostyryl)benzofuran hydrochloride

Chemical Property:

Purity/Quality:

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Technology Process of (E)-6-(2-(3-oxazolidinyl)ethoxy)-2-(4-dimethylaminostyryl)benzofuran hydrochloride

There total 6 articles about (E)-6-(2-(3-oxazolidinyl)ethoxy)-2-(4-dimethylaminostyryl)benzofuran hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1462469-84-6
(E)-6-(2-(3-oxazolidinyl)ethoxy)-2-(4-dimethylaminostyryl)benzofuran

: 1462470-08-1
(E)-6-(2-(3-oxazolidinyl)ethoxy)-2-(4-dimethylaminostyryl)benzofuran hydrochloride

Guidance literature:: With hydrogenchloride; In Dimethyl ether; ethyl acetate; at 20 ℃; for 4.5h;

Reference yield:

: 50551-57-0
ethyl 6-methoxybenzo[b]furan-2-carboxylate

: 1462470-08-1
(E)-6-(2-(3-oxazolidinyl)ethoxy)-2-(4-dimethylaminostyryl)benzofuran hydrochloride

Guidance literature:: Multi-step reaction with 6 steps

1.1: sodium tetrahydroborate / tetrahydrofuran / 1 h / Reflux

1.2: Reflux

2.1: acetonitrile / 1 h / Reflux

3.1: potassium carbonate / methanol / 0.5 h / 20 °C

3.2: 3 h / Darkness

4.1: sodium thioethylate / N,N-dimethyl-formamide / 1 h / Reflux

5.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 3 h / 20 °C

6.1: hydrogenchloride / ethyl acetate; Dimethyl ether / 4.5 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; sodium thioethylate; In tetrahydrofuran; methanol; Dimethyl ether; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;

Reference yield:

: 673-22-3
2-Hydroxy-4-methoxybenzaldehyde

: 1462470-08-1
(E)-6-(2-(3-oxazolidinyl)ethoxy)-2-(4-dimethylaminostyryl)benzofuran hydrochloride

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 20 °C / Large scale

1.2: 3 h / 175 °C / Large scale

2.1: sodium tetrahydroborate / tetrahydrofuran / 1 h / Reflux

2.2: Reflux

3.1: acetonitrile / 1 h / Reflux

4.1: potassium carbonate / methanol / 0.5 h / 20 °C

4.2: 3 h / Darkness

5.1: sodium thioethylate / N,N-dimethyl-formamide / 1 h / Reflux

6.1: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 3 h / 20 °C

7.1: hydrogenchloride / ethyl acetate; Dimethyl ether / 4.5 h / 20 °C

With hydrogenchloride; sodium tetrahydroborate; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; sodium thioethylate; In tetrahydrofuran; methanol; Dimethyl ether; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;