N-(2-tert-butoxycarbonylamino-phenyl)-5-methoxy-isophthalamic acid methyl ester

Base Information

Chemical Name:N-(2-tert-butoxycarbonylamino-phenyl)-5-methoxy-isophthalamic acid methyl ester
CAS No.:1257657-34-3
Molecular Formula:C₂₁H₂₄N₂O₆
Molecular Weight:400.431
Hs Code.:

Synonyms:N-(2-tert-butoxycarbonylamino-phenyl)-5-methoxy-isophthalamic acid methyl ester

Suppliers and Price of N-(2-tert-butoxycarbonylamino-phenyl)-5-methoxy-isophthalamic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of N-(2-tert-butoxycarbonylamino-phenyl)-5-methoxy-isophthalamic acid methyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Technology Process of N-(2-tert-butoxycarbonylamino-phenyl)-5-methoxy-isophthalamic acid methyl ester

There total 1 articles about N-(2-tert-butoxycarbonylamino-phenyl)-5-methoxy-isophthalamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 146651-75-4
tert–butyl (2–aminophenyl)carbamate

: 71590-08-4
5-methoxy-isophthalic acid monomethyl ester

: 1257657-34-3
N-(2-tert-butoxycarbonylamino-phenyl)-5-methoxy-isophthalamic acid methyl ester

Guidance literature:: 5-methoxy-isophthalic acid monomethyl ester; With N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; for 0.333333h;

tert–butyl (2–aminophenyl)carbamate; In tetrahydrofuran; for 18h;

Reference yield: 78.0%

: 1257657-34-3
N-(2-tert-butoxycarbonylamino-phenyl)-5-methoxy-isophthalamic acid methyl ester

: 1257657-58-1
[2-(3-hydroxymethyl-5-methoxy-benzoylamino)-phenyl]carbamic acid tert-butyl ester

Guidance literature:: With diisobutylaluminium hydride; In tetrahydrofuran; dichloromethane; at -78 - 0 ℃;

Reference yield:

: 1257657-34-3
N-(2-tert-butoxycarbonylamino-phenyl)-5-methoxy-isophthalamic acid methyl ester

: 1257657-37-6
(S)-methyl 3-(2-(3-methoxy-5-vinylbenzamido)phenylcarbamoyl)-3-(allyloxy)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / dichloromethane; tetrahydrofuran / -78 - 0 °C

2: dipyridinium dichromate / dichloromethane / 18 h / 20 °C / Inert atmosphere

3: hydrogenchloride / 1,4-dioxane / 4 h / 0 °C

4: N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / tetrahydrofuran / 0.33 h

With hydrogenchloride; dipyridinium dichromate; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; 1,4-dioxane; dichloromethane;