(S)-methyl 3-(2-(3-methoxy-5-vinylbenzamido)phenylcarbamoyl)-3-(allyloxy)propanoate

Base Information

Chemical Name:(S)-methyl 3-(2-(3-methoxy-5-vinylbenzamido)phenylcarbamoyl)-3-(allyloxy)propanoate
CAS No.:1257657-37-6
Molecular Formula:C₂₈H₃₄N₂O₆
Molecular Weight:494.588
Hs Code.:

Synonyms:(S)-methyl 3-(2-(3-methoxy-5-vinylbenzamido)phenylcarbamoyl)-3-(allyloxy)propanoate

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Chemical Property of (S)-methyl 3-(2-(3-methoxy-5-vinylbenzamido)phenylcarbamoyl)-3-(allyloxy)propanoate

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Technology Process of (S)-methyl 3-(2-(3-methoxy-5-vinylbenzamido)phenylcarbamoyl)-3-(allyloxy)propanoate

There total 4 articles about (S)-methyl 3-(2-(3-methoxy-5-vinylbenzamido)phenylcarbamoyl)-3-(allyloxy)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1257657-18-3
(S)-2-allyloxyoctanedioic acid 8-methyl ester

: 1257657-59-2
2-(3-methoxy-5-vinyl-benzoylamino)-phenyl-ammonium chloride

: 1257657-37-6
(S)-methyl 3-(2-(3-methoxy-5-vinylbenzamido)phenylcarbamoyl)-3-(allyloxy)propanoate

Guidance literature:: (S)-2-allyloxyoctanedioic acid 8-methyl ester; With N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; at 20 ℃; for 0.25h; Cooling with ice; Inert atmosphere;

2-(3-methoxy-5-vinyl-benzoylamino)-phenyl-ammonium chloride; In tetrahydrofuran; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm101092u

Reference yield:

: 1257657-34-3
N-(2-tert-butoxycarbonylamino-phenyl)-5-methoxy-isophthalamic acid methyl ester

: 1257657-37-6
(S)-methyl 3-(2-(3-methoxy-5-vinylbenzamido)phenylcarbamoyl)-3-(allyloxy)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / dichloromethane; tetrahydrofuran / -78 - 0 °C

2: dipyridinium dichromate / dichloromethane / 18 h / 20 °C / Inert atmosphere

3: hydrogenchloride / 1,4-dioxane / 4 h / 0 °C

4: N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / tetrahydrofuran / 0.33 h

With hydrogenchloride; dipyridinium dichromate; diisobutylaluminium hydride; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; 1,4-dioxane; dichloromethane;

Reference yield:

: 1257657-58-1
[2-(3-hydroxymethyl-5-methoxy-benzoylamino)-phenyl]carbamic acid tert-butyl ester

: 1257657-37-6
(S)-methyl 3-(2-(3-methoxy-5-vinylbenzamido)phenylcarbamoyl)-3-(allyloxy)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: dipyridinium dichromate / dichloromethane / 18 h / 20 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane / 4 h / 0 °C

3: N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one / tetrahydrofuran / 0.33 h

With hydrogenchloride; dipyridinium dichromate; N-ethyl-N,N-diisopropylamine; 3-[(diethoxyphosphinyl)oxy]-1,2,3-benzotriazin-4(3H)-one; In tetrahydrofuran; 1,4-dioxane; dichloromethane;