1,3-dipropyl-7-o-nitrobenzyl-8-[5,6-exo-epoxy-(1S,2S)-norbornan-2-yl]xanthine

Base Information

Chemical Name:1,3-dipropyl-7-o-nitrobenzyl-8-[5,6-exo-epoxy-(1S,2S)-norbornan-2-yl]xanthine
CAS No.:638132-97-5
Molecular Formula:C₂₅H₂₉N₅O₅
Molecular Weight:479.536
Hs Code.:

Synonyms:1,3-dipropyl-7-o-nitrobenzyl-8-[5,6-exo-epoxy-(1S,2S)-norbornan-2-yl]xanthine

Suppliers and Price of 1,3-dipropyl-7-o-nitrobenzyl-8-[5,6-exo-epoxy-(1S,2S)-norbornan-2-yl]xanthine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1,3-dipropyl-7-o-nitrobenzyl-8-[5,6-exo-epoxy-(1S,2S)-norbornan-2-yl]xanthine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1,3-dipropyl-7-o-nitrobenzyl-8-[5,6-exo-epoxy-(1S,2S)-norbornan-2-yl]xanthine

There total 4 articles about 1,3-dipropyl-7-o-nitrobenzyl-8-[5,6-exo-epoxy-(1S,2S)-norbornan-2-yl]xanthine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 638132-96-4
1,3-dipropyl-7-o-nitrobenzyl-8-[(1S,2S)-5-norbornen-2-yl]xanthine

: 638132-97-5
1,3-dipropyl-7-o-nitrobenzyl-8-[5,6-exo-epoxy-(1S,2S)-norbornan-2-yl]xanthine

Guidance literature:: With peracetic acid; In dichloromethane; at 20 ℃; for 16h;
DOI:10.1081/SCC-120021980

Reference yield:

: 120-74-1,934-30-5,1195-12-6,20507-53-3,58001-99-3,67999-50-2,67999-53-5,74645-32-2,108266-75-7
(1S,2S,4S)-bicyclo[2.2.1]hept-5-ene-2-carboxylic acid

: 638132-97-5
1,3-dipropyl-7-o-nitrobenzyl-8-[5,6-exo-epoxy-(1S,2S)-norbornan-2-yl]xanthine

Guidance literature:: Multi-step reaction with 4 steps

1: oxalyl chloride / CH₂Cl₂ / 2 h / 20 °C

2: 14.5 g / Et₃N / tetrahydrofuran / 20 °C

3: 43 percent / aq. NaOH / methanol / 15 h / Heating

4: 44 percent / peracetic acid / CH₂Cl₂ / 16 h / 20 °C

With peracetic acid; sodium hydroxide; oxalyl dichloride; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1081/SCC-120021980

Reference yield:

: 244622-23-9,214920-46-4,783334-78-1
(-)-(1S,2S)-5-norbornene-2-carboxylic acid chloride

: 638132-97-5
1,3-dipropyl-7-o-nitrobenzyl-8-[5,6-exo-epoxy-(1S,2S)-norbornan-2-yl]xanthine

Guidance literature:: Multi-step reaction with 3 steps

1: 14.5 g / Et₃N / tetrahydrofuran / 20 °C

2: 43 percent / aq. NaOH / methanol / 15 h / Heating

3: 44 percent / peracetic acid / CH₂Cl₂ / 16 h / 20 °C

With peracetic acid; sodium hydroxide; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1081/SCC-120021980