2-propenyl 2,3,4,6-tetra-O-benzyl-α-D-glactopyranoside

Base Information

Chemical Name:2-propenyl 2,3,4,6-tetra-O-benzyl-α-D-glactopyranoside
CAS No.:112344-80-6
Molecular Formula:C₃₇H₄₀O₆
Molecular Weight:580.721
Hs Code.:

Synonyms:2-propenyl 2,3,4,6-tetra-O-benzyl-α-D-glactopyranoside

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Chemical Property of 2-propenyl 2,3,4,6-tetra-O-benzyl-α-D-glactopyranoside

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Technology Process of 2-propenyl 2,3,4,6-tetra-O-benzyl-α-D-glactopyranoside

There total 62 articles about 2-propenyl 2,3,4,6-tetra-O-benzyl-α-D-glactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 107-18-6
allyl alcohol

: 2,3,4,6-tetra-O-benzyl-α,β-D-glucopyranosyl N-trichloroacetylcarbamate

: 6207-45-0,60478-61-7,112344-80-6,126924-14-9,6207-44-9
2-(allyloxy)-3,4,5-tris(benzyloxy)-6-(benzyloxymethyl)-tetrahydro-2H-pyran

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 0 ℃; for 0.1h;
DOI:10.1016/j.carres.2005.07.024

Reference yield: 95.0%

: 194088-19-2
(2R,3R,4S,5R,6S)-3,4,5-tris(benzyloxy)-2-(benzyloxymethyl)-6-(prop-2-ynyloxy)tetrahydro-2H-pyran

: 107-18-6
allyl alcohol

: 6207-44-9,6207-45-0,60478-61-7,112344-80-6,126924-14-9
1-allyl-2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

Guidance literature:: With FeCl₃/C; In acetonitrile; at 60 ℃; for 5h; stereoselective reaction; Inert atmosphere; Green chemistry;
DOI:10.1055/s-0037-1611801

Reference yield: 93.0%

: 74808-09-6
2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

: 107-18-6
allyl alcohol

: 6207-44-9,6207-45-0,60478-61-7,112344-80-6,126924-14-9
1-allyl-2,3,4,6-tetra-O-benzyl-β-D-glucopyranoside

Guidance literature:: 2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate; allyl alcohol; With 1,3-bis(3,5-bis(trifluoro-ethyl)phenyl)thiourea; In dichloromethane; at 20 ℃; for 0.0833333h;

With Bis(p-nitrophenyl) phosphate; In dichloromethane; at 20 ℃; for 0.25h;
DOI:10.1002/anie.201302158