3-({[(2S)-2-amino-3-methoxy-3-oxopropyl]carbamoyl}amino)-5-chloro-4-methylbenzene-1-sulfonic acid

Base Information

Chemical Name:3-({[(2S)-2-amino-3-methoxy-3-oxopropyl]carbamoyl}amino)-5-chloro-4-methylbenzene-1-sulfonic acid
CAS No.:1333219-06-9
Molecular Formula:C₁₂H₁₆ClN₃O₆S
Molecular Weight:365.795
Hs Code.:

Synonyms:3-({[(2S)-2-amino-3-methoxy-3-oxopropyl]carbamoyl}amino)-5-chloro-4-methylbenzene-1-sulfonic acid

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Chemical Property of 3-({[(2S)-2-amino-3-methoxy-3-oxopropyl]carbamoyl}amino)-5-chloro-4-methylbenzene-1-sulfonic acid

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Technology Process of 3-({[(2S)-2-amino-3-methoxy-3-oxopropyl]carbamoyl}amino)-5-chloro-4-methylbenzene-1-sulfonic acid

There total 8 articles about 3-({[(2S)-2-amino-3-methoxy-3-oxopropyl]carbamoyl}amino)-5-chloro-4-methylbenzene-1-sulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.3%

: 6387-27-5
3-amino-5-chloro-4-methylbenzenesulfonic acid

: 61040-20-8
(S)-methyl 3-amino-2-((tert-butoxycarbonyl)amino)propanoate

: 1885-14-9
phenyl chloroformate

: 1333219-06-9
3-({[(2S)-2-amino-3-methoxy-3-oxopropyl]carbamoyl}amino)-5-chloro-4-methylbenzene-1-sulfonic acid

Guidance literature:: 3-amino-5-chloro-4-methylbenzenesulfonic acid; phenyl chloroformate; With pyridine; In acetonitrile; at 25 ℃; for 0.5h;

(S)-methyl 3-amino-2-((tert-butoxycarbonyl)amino)propanoate; With triethylamine; In methanesulfonic acid; at 50 ℃; for 4h;

Reference yield:

: C₂₁H₂₄ClN₃O₇S*C₆H₁₅N

: 1333219-06-9
3-({[(2S)-2-amino-3-methoxy-3-oxopropyl]carbamoyl}amino)-5-chloro-4-methylbenzene-1-sulfonic acid

Guidance literature:: With hydrogen bromide; In acetic acid; at 20 ℃; for 1.16667h;

Reference yield:

: C₁₅H₁₃Cl₂NO₄S

: 61040-20-8
(S)-methyl 3-amino-2-((tert-butoxycarbonyl)amino)propanoate

: 1333219-06-9
3-({[(2S)-2-amino-3-methoxy-3-oxopropyl]carbamoyl}amino)-5-chloro-4-methylbenzene-1-sulfonic acid

Guidance literature:: C₁₅H₁₃Cl₂NO₄S; (S)-methyl 3-amino-2-((tert-butoxycarbonyl)amino)propanoate; With triethylamine; In acetonitrile; at 40 ℃; for 2h;

In methanesulfonic acid; at 50 ℃; for 3.5h;