Bis(trifluormethyl)phosphinigsaeure-trifluoressigsaeureanhydrid

Base Information

• Chemical Name: Bis(trifluormethyl)phosphinigsaeure-trifluoressigsaeureanhydrid
• CAS No.: 2377-97-1
• Molecular Formula: C₄F₉O₂P
• Molecular Weight: 282.002
• Mol file: 2377-97-1.mol

Synonyms:Bis(trifluormethyl)phosphinigsaeure-trifluoressigsaeureanhydrid

Chemical Property of Bis(trifluormethyl)phosphinigsaeure-trifluoressigsaeureanhydrid

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of Bis(trifluormethyl)phosphinigsaeure-trifluoressigsaeureanhydrid

There total 1 articles about Bis(trifluormethyl)phosphinigsaeure-trifluoressigsaeureanhydrid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

iodo-bis-trifluoromethyl-phosphine (359-64-8) + silver trifluoroacetate (2966-50-9) → Bis(trifluormethyl)phosphinigsaeure-trifluoressigsaeureanhydrid (2377-97-1) + Tetrakis(trifluormethyl)disphosphoxan (2728-67-8) + trifluoroacetic anhydride (407-25-0)

Guidance literature:

byproducts: AgI; below 20°C; further react. in equil.; distn.; main product as medium fraction at 0°C / 55 Torr;

DOI:10.1021/ja01067a014

Reference yield:

Bis(trifluormethyl)phosphinigsaeure-trifluoressigsaeureanhydrid (2377-97-1) → Tetrakis(trifluormethyl)disphosphoxan (2728-67-8) + trifluoroacetic anhydride (407-25-0)

Guidance literature:

at 40 ℃; Equilibrium constant;

DOI:10.1021/ja01067a014

upstream raw materials:

iodo-bis-trifluoromethyl-phosphine

silver trifluoroacetate

Downstream raw materials:

Tetrakis(trifluormethyl)disphosphoxan

trifluoroacetic anhydride