4,4'-(6,6'-dimethylbiphenyl-2,2'-diyl)bis(oxy)bis(methylene)bis(1-benzyl-1H-1,2,3-triazole)

Base Information

Chemical Name:4,4'-(6,6'-dimethylbiphenyl-2,2'-diyl)bis(oxy)bis(methylene)bis(1-benzyl-1H-1,2,3-triazole)
CAS No.:1268524-63-5
Molecular Formula:C₃₄H₃₂N₆O₂
Molecular Weight:556.667
Hs Code.:

Synonyms:4,4'-(6,6'-dimethylbiphenyl-2,2'-diyl)bis(oxy)bis(methylene)bis(1-benzyl-1H-1,2,3-triazole)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4,4'-(6,6'-dimethylbiphenyl-2,2'-diyl)bis(oxy)bis(methylene)bis(1-benzyl-1H-1,2,3-triazole)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 4,4'-(6,6'-dimethylbiphenyl-2,2'-diyl)bis(oxy)bis(methylene)bis(1-benzyl-1H-1,2,3-triazole)

There total 3 articles about 4,4'-(6,6'-dimethylbiphenyl-2,2'-diyl)bis(oxy)bis(methylene)bis(1-benzyl-1H-1,2,3-triazole) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1268524-60-2
2,2'-dimethyl-6,6'-bis(prop-2-ynyloxy)biphenyl

: 622-79-7
benzyl azide

: 1268524-63-5
4,4'-(6,6'-dimethylbiphenyl-2,2'-diyl)bis(oxy)bis(methylene)bis(1-benzyl-1H-1,2,3-triazole)

Guidance literature:: With Cu(I)Cl-(2,4-dimethoxyphenylisonitrile) complex; In water; at 20 ℃; for 6h;
DOI:10.1021/ol103134c

Reference yield:

: 100-39-0
benzyl bromide

: 1268524-63-5
4,4'-(6,6'-dimethylbiphenyl-2,2'-diyl)bis(oxy)bis(methylene)bis(1-benzyl-1H-1,2,3-triazole)

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide / dimethyl sulfoxide / 25 °C

2: Cu(I)Cl-(2,4-dimethoxyphenylisonitrile) complex / water / 6 h / 20 °C

With sodium azide; In water; dimethyl sulfoxide; 2: Huisgen [3+2] dipolar cycloaddition;
DOI:10.1021/ol103134c

Reference yield:

: 32750-01-9
6,6'-dimethyl-2,2'-biphenyldiol

: 1268524-63-5
4,4'-(6,6'-dimethylbiphenyl-2,2'-diyl)bis(oxy)bis(methylene)bis(1-benzyl-1H-1,2,3-triazole)

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / acetone / 16 h / Inert atmosphere; Reflux

2: Cu(I)Cl-(2,4-dimethoxyphenylisonitrile) complex / water / 6 h / 20 °C

With potassium carbonate; In water; acetone; 2: Huisgen [3+2] dipolar cycloaddition;
DOI:10.1021/ol103134c