9-benzoyloxy-1,5-dithiaspiro<5.5>undecane

Base Information

Chemical Name:9-benzoyloxy-1,5-dithiaspiro<5.5>undecane
CAS No.:128432-36-0
Molecular Formula:C₁₆H₂₀O₂S₂
Molecular Weight:308.466
Hs Code.:

Synonyms:9-benzoyloxy-1,5-dithiaspiro<5.5>undecane

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Chemical Property of 9-benzoyloxy-1,5-dithiaspiro<5.5>undecane

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Technology Process of 9-benzoyloxy-1,5-dithiaspiro<5.5>undecane

There total 1 articles about 9-benzoyloxy-1,5-dithiaspiro<5.5>undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 109-80-8
1.3-propanedithiol

: 23510-95-4
4-benzoyloxycyclohexanone

: 128432-36-0
9-benzoyloxy-1,5-dithiaspiro<5.5>undecane

Guidance literature:: With toluene-4-sulfonic acid; In acetic acid; for 1h; Ambient temperature;

Reference yield:

: 128432-36-0
9-benzoyloxy-1,5-dithiaspiro<5.5>undecane

: N-(1,5-Dithia-spiro[5.5]undec-9-ylidene)-N'-phenyl-hydrazine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / 2 M NaOH / tetrahydrofuran / 2 h / Heating

2: 73 percent / pyridine, TFA, DCC / benzene; dimethylsulfoxide / Ambient temperature

3: Na₂CO₃ / ethanol; H₂O / 1 h / Heating

With pyridine; sodium hydroxide; sodium carbonate; dicyclohexyl-carbodiimide; trifluoroacetic acid; In tetrahydrofuran; ethanol; water; dimethyl sulfoxide; benzene;

Reference yield:

: 128432-36-0
9-benzoyloxy-1,5-dithiaspiro<5.5>undecane

: 51145-61-0
1,2,3,4-tetrahydrocarbazol-3-one

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / 2 M NaOH / tetrahydrofuran / 2 h / Heating

2: 73 percent / pyridine, TFA, DCC / benzene; dimethylsulfoxide / Ambient temperature

3: Na₂CO₃ / ethanol; H₂O / 1 h / Heating

4: acetic acid / 0.5 h / 100 °C

5: 65 percent / HgO, HgCl₂ / methanol; H₂O / 2 h / Heating

With pyridine; sodium hydroxide; sodium carbonate; acetic acid; dicyclohexyl-carbodiimide; trifluoroacetic acid; mercury dichloride; mercury(II) oxide; In tetrahydrofuran; methanol; ethanol; water; dimethyl sulfoxide; benzene;