(Z)-3-((R)-2-Hydroxy-1-phenyl-ethylamino)-pent-2-enedioic acid dimethyl ester

Base Information

Chemical Name:(Z)-3-((R)-2-Hydroxy-1-phenyl-ethylamino)-pent-2-enedioic acid dimethyl ester
CAS No.:871331-01-0
Molecular Formula:C₁₅H₁₉NO₅
Molecular Weight:293.32
Hs Code.:

Synonyms:(Z)-3-((R)-2-Hydroxy-1-phenyl-ethylamino)-pent-2-enedioic acid dimethyl ester

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Chemical Property of (Z)-3-((R)-2-Hydroxy-1-phenyl-ethylamino)-pent-2-enedioic acid dimethyl ester

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Technology Process of (Z)-3-((R)-2-Hydroxy-1-phenyl-ethylamino)-pent-2-enedioic acid dimethyl ester

There total 1 articles about (Z)-3-((R)-2-Hydroxy-1-phenyl-ethylamino)-pent-2-enedioic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1830-54-2
3-oxopentanedioic acid dimethyl ester

: 56613-80-0
D-2-phenylglycinol

: 871331-01-0
(Z)-3-((R)-2-Hydroxy-1-phenyl-ethylamino)-pent-2-enedioic acid dimethyl ester

Guidance literature:: In toluene; for 48h; Heating;
DOI:10.1016/j.tetlet.2005.09.114

Reference yield: 83.0%

: 871331-01-0
(Z)-3-((R)-2-Hydroxy-1-phenyl-ethylamino)-pent-2-enedioic acid dimethyl ester

: 871331-02-1
((R)-7-Oxo-3-phenyl-2,3,4,7-tetrahydro-[1,4]oxazepin-5-yl)-acetic acid methyl ester

Guidance literature:: (Z)-3-((R)-2-Hydroxy-1-phenyl-ethylamino)-pent-2-enedioic acid dimethyl ester; With sodium hydride; In tetrahydrofuran; at 20 ℃; for 1h;

With ammonium chloride; In water;
DOI:10.1016/j.tetlet.2005.09.114

Reference yield:

: 871331-01-0
(Z)-3-((R)-2-Hydroxy-1-phenyl-ethylamino)-pent-2-enedioic acid dimethyl ester

: 2-Benzyl-2-((R)-7-oxo-3-phenyl-2,3,4,7-tetrahydro-[1,4]oxazepin-5-yl)-3-phenyl-propionic acid methyl ester

Guidance literature:: (Z)-3-((R)-2-Hydroxy-1-phenyl-ethylamino)-pent-2-enedioic acid dimethyl ester; With sodium hydride;

Bn-X; at 0 ℃; for 1.5h;

With ammonium chloride; In water;
DOI:10.1016/j.tetlet.2005.09.114