Technology Process of 5-methoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl N,N-diethylcarbamate
There total 1 articles about 5-methoxy-2-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl N,N-diethylcarbamate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
(1,5-cyclooctadiene)(methoxy)iridium(I) dimer;
In
hexane;
at 70 ℃;
Inert atmosphere;
Sealed tube;
DOI:10.1021/ol101493m
- Guidance literature:
-
With
sodium carbonate;
In
1,2-dimethoxyethane; water;
at 90 ℃;
for 16h;
DOI:10.3987/COM-12-S(N)131
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium carbonate / 1,2-dimethoxyethane; water / 16 h / 90 °C
2: organic lithium / tetrahydrofuran / Cooling
With
sodium carbonate;
In
tetrahydrofuran; 1,2-dimethoxyethane; water;
1: |Suzuki-Miyaura Coupling;
DOI:10.3987/COM-12-S(N)131
