Phenylmethyl N-<4-(4,5-dihydro-5-oxo-2-phenyl-4-oxazoyl)butyl>carbamate

Base Information

Chemical Name:Phenylmethyl N-<4-(4,5-dihydro-5-oxo-2-phenyl-4-oxazoyl)butyl>carbamate
CAS No.:123003-97-4
Molecular Formula:C₂₁H₂₂N₂O₄
Molecular Weight:366.417
Hs Code.:

Synonyms:Phenylmethyl N-<4-(4,5-dihydro-5-oxo-2-phenyl-4-oxazoyl)butyl>carbamate

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Chemical Property of Phenylmethyl N-<4-(4,5-dihydro-5-oxo-2-phenyl-4-oxazoyl)butyl>carbamate

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Technology Process of Phenylmethyl N-<4-(4,5-dihydro-5-oxo-2-phenyl-4-oxazoyl)butyl>carbamate

There total 6 articles about Phenylmethyl N-<4-(4,5-dihydro-5-oxo-2-phenyl-4-oxazoyl)butyl>carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1946-80-1
Bz-Lys(Z)-OH

: 123003-97-4
Phenylmethyl N-<4-(4,5-dihydro-5-oxo-2-phenyl-4-oxazoyl)butyl>carbamate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 18 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: 70422-07-0,111319-11-0
N^α-benzoyl-N^ε-(benzyloxycarbonyl)lysine

: 123003-97-4
Phenylmethyl N-<4-(4,5-dihydro-5-oxo-2-phenyl-4-oxazoyl)butyl>carbamate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 0 ℃; for 1h;
DOI:10.1055/s-1979-28634

Reference yield:

: 32302-83-3,57705-97-2,67178-46-5,25931-47-9
N-ε-benzyloxycarbonyl lysine

: 123003-97-4
Phenylmethyl N-<4-(4,5-dihydro-5-oxo-2-phenyl-4-oxazoyl)butyl>carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: NaOH / diethyl ether; H₂O / pH=10-12

2: Ac₂O

With sodium hydroxide; acetic anhydride; In diethyl ether; water;
DOI:10.1016/S0040-4039(00)84319-1