of 2,11-dimethoxy-6-(4-methoxyphenyl)triphenylene

Base Information

Chemical Name:of 2,11-dimethoxy-6-(4-methoxyphenyl)triphenylene
CAS No.:1433220-15-5
Molecular Formula:C₂₇H₂₂O₃
Molecular Weight:394.47
Hs Code.:

Synonyms:of 2,11-dimethoxy-6-(4-methoxyphenyl)triphenylene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of of 2,11-dimethoxy-6-(4-methoxyphenyl)triphenylene

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Technology Process of of 2,11-dimethoxy-6-(4-methoxyphenyl)triphenylene

There total 2 articles about of 2,11-dimethoxy-6-(4-methoxyphenyl)triphenylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 136612-96-9
4,4″-dimethoxy-4′-(4-methoxyphenyl)-1,1′:2′,1″-terphenyl

: 1433220-15-5
of 2,11-dimethoxy-6-(4-methoxyphenyl)triphenylene

Guidance literature:: With tetrabutylammonium tetrafluoroborate; trifluoroacetic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 20 ℃; Electrolysis; Inert atmosphere; Schlenk technique;
DOI:10.1002/adsc.201601331

Reference yield:

: 768-60-5
4-methoxyphenylacetylen

: 1433220-15-5
of 2,11-dimethoxy-6-(4-methoxyphenyl)triphenylene

Guidance literature:: Multi-step reaction with 2 steps

1: cobalt(II) bromide; 1,1,3,3-tetramethyl-2-thiourea; zinc; carbon monoxide / toluene / 15 h / 90 °C / Molecular sieve; Schlenk technique

2: methanesulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0.67 h / 0 °C

With methanesulfonic acid; 1,1,3,3-tetramethyl-2-thiourea; carbon monoxide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; cobalt(II) bromide; zinc; In dichloromethane; toluene; 1: |Pauson-Khand Annulation;
DOI:10.1021/jo400570b