C₂₁H₃₆N₂O₄Si

Base Information

Chemical Name:C₂₁H₃₆N₂O₄Si
CAS No.:1376687-56-7
Molecular Formula:C₂₁H₃₆N₂O₄Si
Molecular Weight:408.613
Hs Code.:

C<sub>21</sub>H<sub>36</sub>N<sub>2</sub>O<sub>4</sub>Si

Synonyms:C₂₁H₃₆N₂O₄Si

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Chemical Property of C₂₁H₃₆N₂O₄Si

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Technology Process of C₂₁H₃₆N₂O₄Si

There total 7 articles about C₂₁H₃₆N₂O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1376687-61-4
1-[2,6-dimethoxy-1-((triisopropylsilyloxy)methyl)cyclohexa-2,5-dienyl]propane-2-one

: 1376687-56-7
C₂₁H₃₆N₂O₄Si

Guidance literature:: 1-[2,6-dimethoxy-1-((triisopropylsilyloxy)methyl)cyclohexa-2,5-dienyl]propane-2-one; With 2,2,2-trifluoroethyl trifluoroacetate; lithium hexamethyldisilazane; at -78 ℃; Inert atmosphere;

With p-nitrobenzenesulfonyl azide; triethylamine; at 20 - 40 ℃; Inert atmosphere;
DOI:10.1038/ja.2012.125

Reference yield:

: C₂₃H₃₇F₃O₅Si

: 1376687-56-7
C₂₁H₃₆N₂O₄Si

Guidance literature:: With p-nitrobenzenesulfonyl azide; triethylamine; In tetrahydrofuran; at 20 - 40 ℃; Inert atmosphere;
DOI:10.1021/jo300646j

Reference yield:

: 185385-63-1
C₁₃H₁₈O₄

: 1376687-56-7
C₂₁H₃₆N₂O₄Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: lithium aluminium tetrahydride / diethyl ether / 0 °C / Inert atmosphere

2.1: triethylamine / dichloromethane / 0 °C / Inert atmosphere

3.1: potassium osmate(VI) dihydrate; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 20 °C / Inert atmosphere

4.1: sodium periodate / methanol; water / 0 - 20 °C / Inert atmosphere

5.1: toluene / 4 h / 0 °C / Inert atmosphere

5.2: 0 - 20 °C / Inert atmosphere

6.1: lithium hexamethyldisilazane / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

6.2: 1 h / -78 - 20 °C / Inert atmosphere

7.1: p-nitrobenzenesulfonyl azide; triethylamine / tetrahydrofuran / 20 - 40 °C / Inert atmosphere

With p-nitrobenzenesulfonyl azide; potassium osmate(VI) dihydrate; sodium periodate; lithium aluminium tetrahydride; potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; lithium hexamethyldisilazane; potassium hexacyanoferrate(III); In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; toluene; tert-butyl alcohol; 5.2: Oppenauer oxidation;
DOI:10.1021/jo300646j