N-[1,3-di(tert-butoxycarbonyl)-4-(fur-2-yl)imidazolidin-2-ylidene]-4-ethylaminoaniline

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Chemical Name:N-[1,3-di(tert-butoxycarbonyl)-4-(fur-2-yl)imidazolidin-2-ylidene]-4-ethylaminoaniline
CAS No.:1615250-76-4
Molecular Formula:C₂₅H₃₄N₄O₅
Molecular Weight:470.569
Hs Code.:

Synonyms:N-[1,3-di(tert-butoxycarbonyl)-4-(fur-2-yl)imidazolidin-2-ylidene]-4-ethylaminoaniline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[1,3-di(tert-butoxycarbonyl)-4-(fur-2-yl)imidazolidin-2-ylidene]-4-ethylaminoaniline

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Technology Process of N-[1,3-di(tert-butoxycarbonyl)-4-(fur-2-yl)imidazolidin-2-ylidene]-4-ethylaminoaniline

There total 3 articles about N-[1,3-di(tert-butoxycarbonyl)-4-(fur-2-yl)imidazolidin-2-ylidene]-4-ethylaminoaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1393670-63-7
1,3-di(tert-butoxycarbonyl)-4-(fur-2-yl)imidazolidine-2-thione

: 5840-09-5
4-amino-1-(N-ethylamino)benzene

: 1615250-76-4
N-[1,3-di(tert-butoxycarbonyl)-4-(fur-2-yl)imidazolidin-2-ylidene]-4-ethylaminoaniline

Guidance literature:: With triethylamine; mercury dichloride; In dichloromethane; at 0 - 20 ℃; for 17h;
DOI:10.1016/j.ejmech.2014.05.057

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1615250-76-4
N-[1,3-di(tert-butoxycarbonyl)-4-(fur-2-yl)imidazolidin-2-ylidene]-4-ethylaminoaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h

1.2: 3 h

2.1: mercury dichloride; triethylamine / dichloromethane / 17 h / 0 - 20 °C

With sodium hydride; triethylamine; mercury dichloride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1016/j.ejmech.2014.05.057

Reference yield:

: 64801-77-0
(rac)-4-(furan-2-yl)imidazolidine-2-thione

: 1615250-76-4
N-[1,3-di(tert-butoxycarbonyl)-4-(fur-2-yl)imidazolidin-2-ylidene]-4-ethylaminoaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.25 h

1.2: 3 h

2.1: mercury dichloride; triethylamine / dichloromethane / 17 h / 0 - 20 °C

With sodium hydride; triethylamine; mercury dichloride; In tetrahydrofuran; dichloromethane; mineral oil;
DOI:10.1016/j.ejmech.2014.05.057