methyl O-(2-amino-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-lactate

Base Information

Chemical Name:methyl O-(2-amino-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-lactate
CAS No.:671792-65-7
Molecular Formula:C₃₁H₃₇NO₇
Molecular Weight:535.637
Hs Code.:

Synonyms:methyl O-(2-amino-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-lactate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl O-(2-amino-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-lactate

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Technology Process of methyl O-(2-amino-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-lactate

There total 2 articles about methyl O-(2-amino-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-lactate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 671792-63-5
methyl O-(3,4,6-tri-O-benzyl-2-deoxy-2-nitro-β-D-glucopyranosyl)-L-lactate

: 671792-65-7
methyl O-(2-amino-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-lactate

Guidance literature:: With hydrogen; Raney Ni (T₄); In ethanol; at 20 ℃; for 48h; atmospheric pressure;
DOI:10.1055/s-2003-42494

Reference yield:

: 117136-22-8
3,4,6-tri-O-benzyl-1,2-dideoxy-2-nitro-D-arabino-hex-1-enopyranose

: 671792-65-7
methyl O-(2-amino-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-L-lactate

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / 3 Angstroem molecular sieves; t-BuOK / tetrahydrofuran; toluene / 12 h / 20 °C

2: 78 percent / H₂ / Raney Ni (T₄) / ethanol / 48 h / 20 °C / atmospheric pressure

With 3 A molecular sieve; potassium tert-butylate; hydrogen; Raney Ni (T₄); In tetrahydrofuran; ethanol; toluene; 1: Michael addition;
DOI:10.1055/s-2003-42494