2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(3,4,5-trimethoxybenzoyl)benzenesulfonamide

Base Information

Chemical Name:2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(3,4,5-trimethoxybenzoyl)benzenesulfonamide
CAS No.:1380545-71-0
Molecular Formula:C₂₅H₂₂ClN₃O₇S₂
Molecular Weight:576.051
Hs Code.:

Synonyms:2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(3,4,5-trimethoxybenzoyl)benzenesulfonamide

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Chemical Property of 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(3,4,5-trimethoxybenzoyl)benzenesulfonamide

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Technology Process of 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(3,4,5-trimethoxybenzoyl)benzenesulfonamide

There total 3 articles about 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(3,4,5-trimethoxybenzoyl)benzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 1380545-54-9
2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)benzenesulfonamide

: 118-41-2
Eudesmic acid

: 1380545-71-0
2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(3,4,5-trimethoxybenzoyl)benzenesulfonamide

Guidance literature:: 2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)benzenesulfonamide; Eudesmic acid; With dmap; dicyclohexyl-carbodiimide; In acetonitrile; at 20 ℃; for 20h;

With toluene-4-sulfonic acid; In ethanol; for 0.0833333h; Cooling with ice;
DOI:10.1007/s00706-012-0732-6

Reference yield:

: 1380545-52-7
2,4-dichloro-5-(1,3,4-oxadiazol-2-yl)benzenesulfonamide

: 1380545-71-0
2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(3,4,5-trimethoxybenzoyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: tetrabutylammomium bromide; potassium carbonate / water; acetonitrile / 24 h / 25 °C / Inert atmosphere

2.1: dmap; dicyclohexyl-carbodiimide / acetonitrile / 20 h / 20 °C

2.2: 0.08 h / Cooling with ice

With dmap; tetrabutylammomium bromide; potassium carbonate; dicyclohexyl-carbodiimide; In water; acetonitrile;
DOI:10.1007/s00706-012-0732-6

Reference yield:

: 18648-15-2
2,4-dichloro-5-(carbazoyl)benzenesulfonamide

: 1380545-71-0
2-benzylthio-4-chloro-5-(1,3,4-oxadiazol-2-yl)-N-(3,4,5-trimethoxybenzoyl)benzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: acetic acid / Reflux

2.1: tetrabutylammomium bromide; potassium carbonate / water; acetonitrile / 24 h / 25 °C / Inert atmosphere

3.1: dmap; dicyclohexyl-carbodiimide / acetonitrile / 20 h / 20 °C

3.2: 0.08 h / Cooling with ice

With dmap; tetrabutylammomium bromide; potassium carbonate; dicyclohexyl-carbodiimide; In water; acetic acid; acetonitrile;
DOI:10.1007/s00706-012-0732-6