1,18-bis(2-cyanoethyl)-1,6,13,18-tetrakis[(4-methylphenyl)sulfonyl]-1,6,13,18-tetraazaoctadeca-3,8,10,15-tetrayne

Base Information

Chemical Name:1,18-bis(2-cyanoethyl)-1,6,13,18-tetrakis[(4-methylphenyl)sulfonyl]-1,6,13,18-tetraazaoctadeca-3,8,10,15-tetrayne
CAS No.:1238279-37-2
Molecular Formula:C₄₈H₄₈N₆O₈S₄
Molecular Weight:965.209
Hs Code.:

Synonyms:1,18-bis(2-cyanoethyl)-1,6,13,18-tetrakis[(4-methylphenyl)sulfonyl]-1,6,13,18-tetraazaoctadeca-3,8,10,15-tetrayne

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Chemical Property of 1,18-bis(2-cyanoethyl)-1,6,13,18-tetrakis[(4-methylphenyl)sulfonyl]-1,6,13,18-tetraazaoctadeca-3,8,10,15-tetrayne

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Technology Process of 1,18-bis(2-cyanoethyl)-1,6,13,18-tetrakis[(4-methylphenyl)sulfonyl]-1,6,13,18-tetraazaoctadeca-3,8,10,15-tetrayne

There total 1 articles about 1,18-bis(2-cyanoethyl)-1,6,13,18-tetrakis[(4-methylphenyl)sulfonyl]-1,6,13,18-tetraazaoctadeca-3,8,10,15-tetrayne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 1238279-12-3
1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazanona-3,8-diyne

: 1238279-37-2
1,18-bis(2-cyanoethyl)-1,6,13,18-tetrakis[(4-methylphenyl)sulfonyl]-1,6,13,18-tetraazaoctadeca-3,8,10,15-tetrayne

Guidance literature:: With copper(l) iodide; triethylamine; palladium dichloride; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.200901318

Reference yield: 88.0%

: 1238279-37-2
1,18-bis(2-cyanoethyl)-1,6,13,18-tetrakis[(4-methylphenyl)sulfonyl]-1,6,13,18-tetraazaoctadeca-3,8,10,15-tetrayne

: 1238279-40-7
C₄₈H₄₈N₆O₈S₄

Guidance literature:: With Wilkinson's catalyst; In dimethyl sulfoxide; at 90 ℃; for 0.166667h; Microwave irradiation; Inert atmosphere; Sealed vial;
DOI:10.1002/ejoc.200901318