1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazanona-3,8-diyne

Base Information

Chemical Name:1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazanona-3,8-diyne
CAS No.:1238279-12-3
Molecular Formula:C₂₄H₂₅N₃O₄S₂
Molecular Weight:483.612
Hs Code.:

Synonyms:1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazanona-3,8-diyne

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazanona-3,8-diyne

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Technology Process of 1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazanona-3,8-diyne

There total 1 articles about 1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazanona-3,8-diyne which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1238279-18-9
N,N'-bis[(4-methylphenyl)sulfonyl]-N'-(2-cyanoethyl)-2-butyne-1,4-diamine

: 106-96-7
propargyl bromide

: 1238279-12-3
1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazanona-3,8-diyne

Guidance literature:: With potassium carbonate; In acetonitrile; for 1h; Reflux;
DOI:10.1002/ejoc.200901318

Reference yield: 73.0%

: 1238279-12-3
1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazanona-3,8-diyne

: 1238279-26-9
C₂₄H₂₅N₃O₄S₂

Guidance literature:: With Wilkinson's catalyst; In chlorobenzene; toluene; at 90 ℃; for 0.5h; Microwave irradiation; Inert atmosphere; Sealed vial;
DOI:10.1002/ejoc.200901318

Reference yield: 37.0%

: 1238279-12-3
1-(2-cyanoethyl)-1,6-bis[(4-methylphenyl)sulfonyl]-1,6-diazanona-3,8-diyne

: 1238279-37-2
1,18-bis(2-cyanoethyl)-1,6,13,18-tetrakis[(4-methylphenyl)sulfonyl]-1,6,13,18-tetraazaoctadeca-3,8,10,15-tetrayne

Guidance literature:: With copper(l) iodide; triethylamine; palladium dichloride; In tetrahydrofuran; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/ejoc.200901318