4-methoxybenzyl 2-(R)-(1-(R)-3-(S)-t-butyldimethylsilyloxymethyl-4-(S)-(3-fluorophenyl)cyclopent-1-yl)-2-(trifluoromethanesulfonyloxy)acetate

Base Information

• Chemical Name: 4-methoxybenzyl 2-(R)-(1-(R)-3-(S)-t-butyldimethylsilyloxymethyl-4-(S)-(3-fluorophenyl)cyclopent-1-yl)-2-(trifluoromethanesulfonyloxy)acetate
• CAS No.: 849204-18-8
• Molecular Formula: C₂₉H₃₈F₄O₇SSi
• Molecular Weight: 634.762

Synonyms:4-methoxybenzyl 2-(R)-(1-(R)-3-(S)-t-butyldimethylsilyloxymethyl-4-(S)-(3-fluorophenyl)cyclopent-1-yl)-2-(trifluoromethanesulfonyloxy)acetate

Chemical Property of 4-methoxybenzyl 2-(R)-(1-(R)-3-(S)-t-butyldimethylsilyloxymethyl-4-(S)-(3-fluorophenyl)cyclopent-1-yl)-2-(trifluoromethanesulfonyloxy)acetate

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Technology Process of 4-methoxybenzyl 2-(R)-(1-(R)-3-(S)-t-butyldimethylsilyloxymethyl-4-(S)-(3-fluorophenyl)cyclopent-1-yl)-2-(trifluoromethanesulfonyloxy)acetate

There total 1 articles about 4-methoxybenzyl 2-(R)-(1-(R)-3-(S)-t-butyldimethylsilyloxymethyl-4-(S)-(3-fluorophenyl)cyclopent-1-yl)-2-(trifluoromethanesulfonyloxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

trifluoromethylsulfonic anhydride (358-23-6) + 4-methoxybenzyl (R)-(1-(R)-3-(S)-t-butyldimethylsilyloxymethyl-4-(S)-(3-fluorophenyl)cyclopent-1-yl)hydroxyacetate (849204-16-6) → 4-methoxybenzyl 2-(R)-(1-(R)-3-(S)-t-butyldimethylsilyloxymethyl-4-(S)-(3-fluorophenyl)cyclopent-1-yl)-2-(trifluoromethanesulfonyloxy)acetate (849204-18-8)

Guidance literature:

With 2,6-dimethylpyridine; In dichloromethane; at -70 - 0 ℃; for 1.33333h;

Reference yield:

2-methyl-2-butylamine (594-39-8) + 4-methoxybenzyl 2-(R)-(1-(R)-3-(S)-t-butyldimethylsilyloxymethyl-4-(S)-(3-fluorophenyl)cyclopent-1-yl)-2-(trifluoromethanesulfonyloxy)acetate (849204-18-8) → 4-methoxybenzyl 2-(S)-(1-(R)-3-(S)-t-butyldimethylsilyloxymethyl-4-(S)-(3-fluorophenyl)cyclopent-1-yl)-2-(1,1-dimethylprop-1-ylamino)acetate (849204-19-9)

Guidance literature:

In 1,2-dichloro-ethane; at 65 ℃; for 20h;

upstream raw materials:

trifluoromethylsulfonic anhydride

4-methoxybenzyl (R)-(1-(R)-3-(S)-t-butyldimethylsilyloxymethyl-4-(S)-(3-fluorophenyl)cyclopent-1-yl)hydroxyacetate

Downstream raw materials:

4-methoxybenzyl 2-(S)-(1-(R)-3-(S)-t-butyldimethylsilyloxymethyl-4-(S)-(3-fluorophenyl)cyclopent-1-yl)-2-(1,1-dimethylprop-1-ylamino)acetate

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