3--1.2-benzo-3.4-cyclohexan-cyclobuten-(1)

Base Information

• Chemical Name: 3--1.2-benzo-3.4-cyclohexan-cyclobuten-(1)
• CAS No.: 101015-59-2
• Molecular Formula: C₁₆H₂₁N
• Molecular Weight: 227.349

Synonyms:3--1.2-benzo-3.4-cyclohexan-cyclobuten-(1)

Chemical Property of 3--1.2-benzo-3.4-cyclohexan-cyclobuten-(1)

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Technology Process of 3--1.2-benzo-3.4-cyclohexan-cyclobuten-(1)

There total 2 articles about 3--1.2-benzo-3.4-cyclohexan-cyclobuten-(1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

o-fluorobromobenzene (1072-85-1) + 1-(1-Cyclohexen-1-yl)pyrrolidine (1125-99-1) → (RS)-2-phenylcyclohexanone (1444-65-1) + 3--1.2-benzo-3.4-cyclohexan-cyclobuten-(1) (101015-59-2) + 1-(1-Phenyl-cyclohex-2-enyl)-pyrrolidine (141346-32-9)

Guidance literature:

Yield given. Multistep reaction. Yields of byproduct given;

DOI:10.1021/jo00040a016

Reference yield:

o-fluorobromobenzene (1072-85-1) + 1-(1-Cyclohexen-1-yl)pyrrolidine (1125-99-1) → 3--1.2-benzo-3.4-cyclohexan-cyclobuten-(1) (101015-59-2) + 6-phenyl-1-pyrrolidinocyclohexene (26974-24-3) + 1-(1-Phenyl-cyclohex-2-enyl)-pyrrolidine (141346-32-9)

Guidance literature:

Mechanism; Product distribution; multistep reaction; also with hydrolysis;

DOI:10.1021/jo00040a016

upstream raw materials:

o-fluorobromobenzene

1-(1-Cyclohexen-1-yl)pyrrolidine

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