(2'E,6'E)-Essigsaeure-<3',7',11'-trimethyl-9'-(p-tolylsulfonyl)-2',6',10'-dodecatrien-1'yl>ester

Base Information

Chemical Name:(2'E,6'E)-Essigsaeure-<3',7',11'-trimethyl-9'-(p-tolylsulfonyl)-2',6',10'-dodecatrien-1'yl>ester
CAS No.:103793-10-8
Molecular Formula:C₂₄H₃₄O₄S
Molecular Weight:418.598
Hs Code.:

Synonyms:(2'E,6'E)-Essigsaeure-<3',7',11'-trimethyl-9'-(p-tolylsulfonyl)-2',6',10'-dodecatrien-1'yl>ester

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Chemical Property of (2'E,6'E)-Essigsaeure-<3',7',11'-trimethyl-9'-(p-tolylsulfonyl)-2',6',10'-dodecatrien-1'yl>ester

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Technology Process of (2'E,6'E)-Essigsaeure-<3',7',11'-trimethyl-9'-(p-tolylsulfonyl)-2',6',10'-dodecatrien-1'yl>ester

There total 2 articles about (2'E,6'E)-Essigsaeure-<3',7',11'-trimethyl-9'-(p-tolylsulfonyl)-2',6',10'-dodecatrien-1'yl>ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 37905-03-6
8-hydroxygeranyl acetate

: 103793-10-8
(2'E,6'E)-Essigsaeure-<3',7',11'-trimethyl-9'-(p-tolylsulfonyl)-2',6',10'-dodecatrien-1'yl>ester

Guidance literature:: Multi-step reaction with 2 steps

1: PBr₃ / diethyl ether / 0.33 h / -25 °C

2: BuLi, N,N'-dimethyl-N,N'-propyleneurea / hexane; tetrahydrofuran / 1.) -78 deg C, 1 h; 2.) -50 deg C, 1 h

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; n-butyllithium; phosphorus tribromide; In tetrahydrofuran; diethyl ether; hexane;
DOI:10.1002/hlca.19850680604

Reference yield:

: 37905-04-7
(2E,6E)-8-bromo-3,7-dimethylocta-2,6-dienyl acetate

: 15543-64-3
prenyl tolyl sulfone

: 103793-10-8
(2'E,6'E)-Essigsaeure-<3',7',11'-trimethyl-9'-(p-tolylsulfonyl)-2',6',10'-dodecatrien-1'yl>ester

Guidance literature:: With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; n-butyllithium; In tetrahydrofuran; hexane; Yield given; 1.) -78 deg C, 1 h; 2.) -50 deg C, 1 h;
DOI:10.1002/hlca.19850680604

Reference yield:

: 103793-10-8
(2'E,6'E)-Essigsaeure-<3',7',11'-trimethyl-9'-(p-tolylsulfonyl)-2',6',10'-dodecatrien-1'yl>ester

: 106-28-5
Farnesol

Guidance literature:: Multi-step reaction with 2 steps

1: KOH / diethyl ether; methanol / 1 h / Ambient temperature

2: Na, dibenzo<18>crown-6 / liquid ammonia; tetrahydrofuran / 0.03 h

With potassium hydroxide; dibenzo-18-crown-6; sodium; In tetrahydrofuran; methanol; diethyl ether; ammonia;
DOI:10.1002/hlca.19850680604