C₁₀H₉Br

Base Information

• Chemical Name: C₁₀H₉Br
• CAS No.: 1554177-90-0
• Molecular Formula: C₁₀H₉Br
• Molecular Weight: 209.085
• Mol file: 1554177-90-0.mol

Synonyms:C₁₀H₉Br

Chemical Property of C₁₀H₉Br

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of C₁₀H₉Br

There total 2 articles about C₁₀H₉Br which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C10H9BrN4O2S → C10H9Br (1554177-90-0)

Guidance literature:

With lithium tert-butoxide; In 1,4-dioxane; at 120 ℃; for 3h; Inert atmosphere;

DOI:10.1002/anie.202107356

Reference yield:

C10H10BrN → C10H9Br (1554177-90-0)

Guidance literature:

Multi-step reaction with 2 steps

1: sulfonyl Azide; 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 2 h

2: lithium tert-butoxide / 1,4-dioxane / 3 h / 120 °C / Inert atmosphere

With sulfonyl Azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium tert-butoxide; In 1,4-dioxane; dichloromethane;

DOI:10.1002/anie.202107356

Reference yield: 68.0%

N,N-dibenzyl-O-benzoylhydroxylamine (52742-32-2) + C10H9Br (1554177-90-0) + bis(pinacol)diborane (73183-34-3) → (1R*,2S*)-N,N-dibenzyl-2-(4-bromophenyl)-1-[(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)methyl]cyclopropan-1-amine

Guidance literature:

With o-phenylenebis(diphenylphosphine); copper(l) chloride; lithium tert-butoxide; In 1,4-dioxane; at 20 ℃; for 4h; diastereoselective reaction; Inert atmosphere;

DOI:10.1021/ol5001507