4-(m-ethylphenyl)cubyl iodide

Base Information

Chemical Name:4-(m-ethylphenyl)cubyl iodide
CAS No.:226896-76-0
Molecular Formula:C₁₆H₁₅I
Molecular Weight:334.2
Hs Code.:

Synonyms:4-(m-ethylphenyl)cubyl iodide

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Chemical Property of 4-(m-ethylphenyl)cubyl iodide

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Technology Process of 4-(m-ethylphenyl)cubyl iodide

There total 2 articles about 4-(m-ethylphenyl)cubyl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 97229-08-8
1,4-diiodocubane

: C₈H₉Li

: 226896-76-0
4-(m-ethylphenyl)cubyl iodide

Guidance literature:: In diethyl ether; pentane; for 0.666667h; Ambient temperature;
DOI:10.1021/ja983441f

Reference yield:

: 32846-66-5
cubane-1,4-dicarboxylic acid

: 226896-76-0
4-(m-ethylphenyl)cubyl iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / I₂, iodobenzene diacetate / benzene / 6 h / Heating

2: 70 percent / pentane; diethyl ether / 0.67 h / Ambient temperature

With [bis(acetoxy)iodo]benzene; iodine; In diethyl ether; pentane; benzene;
DOI:10.1021/ja983441f

Reference yield:

: 97229-08-8
1,4-diiodocubane

: 226896-76-0
4-(m-ethylphenyl)cubyl iodide

: 4-(3-ethyl-phenyl)-4'-iodo-[1,1']bicubanyl

: 4''-(3-ethyl-phenyl)-4-iodo-[1,1';4',1'']tercubane

Guidance literature:: With iodine; tert.-butyl lithium; Multistep reaction; 1.) diethyl ether, pentane, a) -70 deg C, 10 min, b) 0 deg C, 30 min, 2.) diethyl ether, pentane, RT, 20 min;
DOI:10.1021/ja983441f