((1R,2S)-4,4-Bis-ethylsulfanyl-2-methoxymethoxy-1-methyl-butoxy)-tert-butyl-diphenyl-silane

Base Information

Chemical Name:((1R,2S)-4,4-Bis-ethylsulfanyl-2-methoxymethoxy-1-methyl-butoxy)-tert-butyl-diphenyl-silane
CAS No.:86203-36-3
Molecular Formula:C₂₇H₄₂O₃S₂Si
Molecular Weight:506.846
Hs Code.:

Synonyms:((1R,2S)-4,4-Bis-ethylsulfanyl-2-methoxymethoxy-1-methyl-butoxy)-tert-butyl-diphenyl-silane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ((1R,2S)-4,4-Bis-ethylsulfanyl-2-methoxymethoxy-1-methyl-butoxy)-tert-butyl-diphenyl-silane

Chemical Property:

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Technology Process of ((1R,2S)-4,4-Bis-ethylsulfanyl-2-methoxymethoxy-1-methyl-butoxy)-tert-butyl-diphenyl-silane

There total 1 articles about ((1R,2S)-4,4-Bis-ethylsulfanyl-2-methoxymethoxy-1-methyl-butoxy)-tert-butyl-diphenyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67320-20-1,83692-41-5,94292-91-8,64722-95-8
1-(2,2-dimethyl-[1,3]dioxolan-4-yl)-3,3-bis-ethylsulfanyl-propan-1-ol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 86203-36-3
((1R,2S)-4,4-Bis-ethylsulfanyl-2-methoxymethoxy-1-methyl-butoxy)-tert-butyl-diphenyl-silane

Guidance literature:: Yield given. Multistep reaction;

Reference yield: 83.0%

: 86203-36-3
((1R,2S)-4,4-Bis-ethylsulfanyl-2-methoxymethoxy-1-methyl-butoxy)-tert-butyl-diphenyl-silane

: 86203-37-4
(3S,4R)-4-(tert-Butyl-diphenyl-silanyloxy)-3-methoxymethoxy-pentanal

Guidance literature:: With bromine; sodium hydrogencarbonate; In diethyl ether; at 5 ℃;

Reference yield:

: 86203-36-3
((1R,2S)-4,4-Bis-ethylsulfanyl-2-methoxymethoxy-1-methyl-butoxy)-tert-butyl-diphenyl-silane

: 86203-40-9
(Z)-(3S,9S,10R)-2-((2S,5R,6R)-6-tert-Butoxy-5-methyl-tetrahydro-pyran-2-yl)-10-(tert-butyl-diphenyl-silanyloxy)-9-methoxymethoxy-2-methyl-undec-6-en-3-ol

Guidance literature:: Multi-step reaction with 8 steps

1: 83 percent / Br₂, aqueous NaHCO₃ / diethyl ether / 5 °C

2: 75 percent / 40percent HMPA / tetrahydrofuran

3: 97 percent / 2.5percent HCl / methanol / 0 - 20 °C

4: 87 percent / Bu₃P / CH₂Cl₂ / Ambient temperature

5: 97 percent / KHSO₅ / methanol; H₂O / 0 - 20 °C

6: 95 percent / 10percent HMPA, LDA / tetrahydrofuran / -78 °C

7: 1.) Collins; 2.) Al(Hg) / 2.) 10percent aqueous THF, r.t.

8: NaBH₄ / aq. ethanol / Ambient temperature

With hydrogenchloride; N,N,N,N,N,N-hexamethylphosphoric triamide; sodium tetrahydroborate; aluminum amalgam; potassium peroxomonosulfate; tributylphosphine; bromine; sodium hydrogencarbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water;