C₃₀H₄₈O₃Si

Base Information

Chemical Name:C₃₀H₄₈O₃Si
CAS No.:1375412-57-9
Molecular Formula:C₃₀H₄₈O₃Si
Molecular Weight:484.795
Hs Code.:

C<sub>30</sub>H<sub>48</sub>O<sub>3</sub>Si

Synonyms:C₃₀H₄₈O₃Si

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Chemical Property of C₃₀H₄₈O₃Si

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Technology Process of C₃₀H₄₈O₃Si

There total 11 articles about C₃₀H₄₈O₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1375412-52-4
C₃₃H₅₄O₂S₂Si

: 1375412-57-9
C₃₀H₄₈O₃Si

Guidance literature:: With 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate; In water; acetone; at 0 ℃; for 0.00277778 - 0.00416667h;
DOI:10.1002/anie.201108692

Reference yield:

: 105-87-3,8022-83-1
3,7-dimethyl-2E,6-octadien-1-yl acetate

: 1375412-57-9
C₃₀H₄₈O₃Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C

2.1: copper(l) iodide / tetrahydrofuran; dimethyl sulfate / 3 h / -30 °C

3.1: sodium periodate / tetrahydrofuran; water / 6 h / 20 °C

4.1: N-chloro-succinimide; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt / acetonitrile / 2.5 h / 0 °C

4.2: 0.5 h

5.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

5.2: 1 h / -50 - -45 °C

5.3: 2 h / -70 - 0 °C

6.1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

With 2,6-dimethylpyridine; sodium periodate; N-chloro-succinimide; N-Bromosuccinimide; copper(l) iodide; n-butyllithium; (2R,5S)-2-tert-butyl 3,5-dimethylimidazolidin-4-one trifluoroacetic acid salt; silver perchlorate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; hexane; dichloromethane; water; acetone; dimethyl sulfate; acetonitrile; 5.3: Brook rearrangement;
DOI:10.1002/anie.201108692

Reference yield:

: 758692-16-9
(E)-2,2-dimethyl-3-(3-methyl-5-phenylpent-3-enyl)oxirane

: 1375412-57-9
C₃₀H₄₈O₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium periodate / tetrahydrofuran; water / 7.5 h / 20 °C

2.1: sodium hydride / tetrahydrofuran; dimethyl sulfoxide; mineral oil / 1 h / 0 - 20 °C / Inert atmosphere

3.1: (1R,2R)-(-)-N,N'-bis(3,5-di-tert-butylsalicydene)-1,2-cyclohexanediaminocobalt(II); water; acetic acid / tetrahydrofuran / 17.5 h / 20 °C

4.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / 0 - 20 °C

4.2: 1 h / -50 - -45 °C

4.3: 2 h / -70 - 0 °C

5.1: 2,6-dimethylpyridine; N-Bromosuccinimide; silver perchlorate / water; acetone / 0 - 0 h / 0 °C

With 2,6-dimethylpyridine; sodium periodate; N-Bromosuccinimide; (1R,2R)-(-)-N,N'-bis(3,5-di-tert-butylsalicydene)-1,2-cyclohexanediaminocobalt(II); n-butyllithium; water; silver perchlorate; sodium hydride; acetic acid; In tetrahydrofuran; hexane; water; dimethyl sulfoxide; acetone; mineral oil; 2.1: Corey-Chaykovsky reaction / 3.1: Jacobsen hydrolytic kinetic resolution / 4.3: Brook rearrangement;
DOI:10.1002/anie.201108692