(2Z,5Z)-N-[5-({2-[(2,4-dimethylphenyl)azamethylene]-4-oxo(1,3-thiazolidin-5-ylidene)}methyl)(1,3-thiazol-2-yl)](1-methyl(4-piperidyl))carboxamide

Base Information

Chemical Name:(2Z,5Z)-N-[5-({2-[(2,4-dimethylphenyl)azamethylene]-4-oxo(1,3-thiazolidin-5-ylidene)}methyl)(1,3-thiazol-2-yl)](1-methyl(4-piperidyl))carboxamide
CAS No.:1253209-07-2
Molecular Formula:C₂₂H₂₅N₅O₂S₂
Molecular Weight:455.605
Hs Code.:

Synonyms:(2Z,5Z)-N-[5-({2-[(2,4-dimethylphenyl)azamethylene]-4-oxo(1,3-thiazolidin-5-ylidene)}methyl)(1,3-thiazol-2-yl)](1-methyl(4-piperidyl))carboxamide

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Chemical Property of (2Z,5Z)-N-[5-({2-[(2,4-dimethylphenyl)azamethylene]-4-oxo(1,3-thiazolidin-5-ylidene)}methyl)(1,3-thiazol-2-yl)](1-methyl(4-piperidyl))carboxamide

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Technology Process of (2Z,5Z)-N-[5-({2-[(2,4-dimethylphenyl)azamethylene]-4-oxo(1,3-thiazolidin-5-ylidene)}methyl)(1,3-thiazol-2-yl)](1-methyl(4-piperidyl))carboxamide

There total 3 articles about (2Z,5Z)-N-[5-({2-[(2,4-dimethylphenyl)azamethylene]-4-oxo(1,3-thiazolidin-5-ylidene)}methyl)(1,3-thiazol-2-yl)](1-methyl(4-piperidyl))carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68947-43-3
1-methylpiperidine-4-carboxylic acid

: 1253209-07-2
(2Z,5Z)-N-[5-({2-[(2,4-dimethylphenyl)azamethylene]-4-oxo(1,3-thiazolidin-5-ylidene)}methyl)(1,3-thiazol-2-yl)](1-methyl(4-piperidyl))carboxamide

Guidance literature:: Multi-step reaction with 2 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

2: piperidine / ethanol / Reflux

With piperidine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In ethanol; dichloromethane;

Reference yield:

: 1253116-31-2,340316-40-7
C₁₁H₁₂N₂OS

: 1253116-34-5
C₁₁H₁₅N₃O₂S

: 1253209-07-2
(2Z,5Z)-N-[5-({2-[(2,4-dimethylphenyl)azamethylene]-4-oxo(1,3-thiazolidin-5-ylidene)}methyl)(1,3-thiazol-2-yl)](1-methyl(4-piperidyl))carboxamide

Guidance literature:: With piperidine; In ethanol; Reflux;

Reference yield:

: 498-94-2
isonipecotic acid

: 1253209-07-2
(2Z,5Z)-N-[5-({2-[(2,4-dimethylphenyl)azamethylene]-4-oxo(1,3-thiazolidin-5-ylidene)}methyl)(1,3-thiazol-2-yl)](1-methyl(4-piperidyl))carboxamide

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / 10% palladium on activated charcoal / water / 20 °C / 2250.23 Torr

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

3: piperidine / ethanol / Reflux

With piperidine; hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; 10% palladium on activated charcoal; In ethanol; dichloromethane; water;