Ethanone, 1-[4,5-dihydro-2-methyl-5-(1-propenyl)-3-furanyl]-, [R-(E)]- (9CI)

Base Information

Chemical Name:Ethanone, 1-[4,5-dihydro-2-methyl-5-(1-propenyl)-3-furanyl]-, [R-(E)]- (9CI)
CAS No.:185317-33-3
Molecular Formula:C₁₀H₁₄O₂
Molecular Weight:166.22
Hs Code.:
Mol file:185317-33-3.mol

Synonyms:Ethanone,1-[4,5-dihydro-2-methyl-5-(1-propenyl)-3-furanyl]-, [R-(E)]- (9CI)

Suppliers and Price of Ethanone, 1-[4,5-dihydro-2-methyl-5-(1-propenyl)-3-furanyl]-, [R-(E)]- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of Ethanone, 1-[4,5-dihydro-2-methyl-5-(1-propenyl)-3-furanyl]-, [R-(E)]- (9CI)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Ethanone, 1-[4,5-dihydro-2-methyl-5-(1-propenyl)-3-furanyl]-, [R-(E)]- (9CI)

There total 9 articles about Ethanone, 1-[4,5-dihydro-2-methyl-5-(1-propenyl)-3-furanyl]-, [R-(E)]- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 2004-70-8,17410-45-6,25212-15-1,64940-84-7
1-methylbuta-1,3-diene

: 123-54-6,81235-32-7
acetylacetone

: 80485-93-4,185317-33-3
2-methyl-3-acetyl-5-(1-propenyl)-4,5-dihydrofuran

Guidance literature:: With copper diacetate; manganese triacetate; In acetic acid; at 60 ℃; for 0.25h;
DOI:10.1007/BF00949477

Reference yield: 46.0%

: 504-60-9,17410-45-6,25212-15-1,64940-84-7
penta-1,3-diene

: 123-54-6,81235-32-7
acetylacetone

: 80485-93-4,185317-33-3
3-acetyl-2-methyl-5-propenyl-4,5-dihydrofuran

Guidance literature:: With ammonium cerium(IV) nitrate; In methanol; cooling;

Reference yield:

: 185317-28-6
Carbonic acid (E)-(S)-5-acetyl-1-methyl-6-oxo-hept-2-enyl ester methyl ester

: 185317-33-3
2-(1-propenyl)-4-acetyl-5-methyl-2,3-dihydrofuran

: 2-(1-propenyl)-4-acetyl-5-methyl-2,3-dihydrofuran

Guidance literature:: With tris(dibenzylideneacetone)dipalladium⁽⁰⁾ chloroform complex; 1,1'-bis-(diphenylphosphino)ferrocene; In tetrahydrofuran; at 60 ℃; for 15h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1021/jo9603901