tert-butyl (4S,5R,1''E)-4-((((4'-bromo-5'-hydroxy-2'-nitrophenyl)(phenyl)methoxy)(hydroxy)phosphoryloxy)methyl)-2,2-dimethyl-5-(pentadec-1''-enyl)oxazolidine-3-carboxylate

Base Information

Chemical Name:tert-butyl (4S,5R,1''E)-4-((((4'-bromo-5'-hydroxy-2'-nitrophenyl)(phenyl)methoxy)(hydroxy)phosphoryloxy)methyl)-2,2-dimethyl-5-(pentadec-1''-enyl)oxazolidine-3-carboxylate
CAS No.:1196664-91-1
Molecular Formula:C₃₉H₅₈BrN₂O₁₀P
Molecular Weight:825.775
Hs Code.:

tert-butyl (4S,5R,1''E)-4-((((4'-bromo-5'-hydroxy-2'-nitrophenyl)(phenyl)methoxy)(hydroxy)phosphoryloxy)methyl)-2,2-dimethyl-5-(pentadec-1''-enyl)oxazolidine-3-carboxylate

Synonyms:tert-butyl (4S,5R,1''E)-4-((((4'-bromo-5'-hydroxy-2'-nitrophenyl)(phenyl)methoxy)(hydroxy)phosphoryloxy)methyl)-2,2-dimethyl-5-(pentadec-1''-enyl)oxazolidine-3-carboxylate

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Chemical Property of tert-butyl (4S,5R,1''E)-4-((((4'-bromo-5'-hydroxy-2'-nitrophenyl)(phenyl)methoxy)(hydroxy)phosphoryloxy)methyl)-2,2-dimethyl-5-(pentadec-1''-enyl)oxazolidine-3-carboxylate

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Technology Process of tert-butyl (4S,5R,1''E)-4-((((4'-bromo-5'-hydroxy-2'-nitrophenyl)(phenyl)methoxy)(hydroxy)phosphoryloxy)methyl)-2,2-dimethyl-5-(pentadec-1''-enyl)oxazolidine-3-carboxylate

There total 10 articles about tert-butyl (4S,5R,1''E)-4-((((4'-bromo-5'-hydroxy-2'-nitrophenyl)(phenyl)methoxy)(hydroxy)phosphoryloxy)methyl)-2,2-dimethyl-5-(pentadec-1''-enyl)oxazolidine-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1196665-00-5
tert-butyl (4S,5R,1E)-4-((((4'-bromo-5'-methoxy-2'-nitrophenyl)(phenyl)methoxy)(methoxy)phosphoryloxy)methyl)-2,2-dimethyl-5-(pentadec-1-enyl)oxazolidine-3-carboxylate

: 1196664-91-1
tert-butyl (4S,5R,1''E)-4-((((4'-bromo-5'-hydroxy-2'-nitrophenyl)(phenyl)methoxy)(hydroxy)phosphoryloxy)methyl)-2,2-dimethyl-5-(pentadec-1''-enyl)oxazolidine-3-carboxylate

Guidance literature:: tert-butyl (4S,5R,1E)-4-((((4'-bromo-5'-methoxy-2'-nitrophenyl)(phenyl)methoxy)(methoxy)phosphoryloxy)methyl)-2,2-dimethyl-5-(pentadec-1-enyl)oxazolidine-3-carboxylate; With pyridine; lithium iodide; Reflux;

With water; ammonium chloride;
DOI:10.1021/jo902076w

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 1196664-91-1
tert-butyl (4S,5R,1''E)-4-((((4'-bromo-5'-hydroxy-2'-nitrophenyl)(phenyl)methoxy)(hydroxy)phosphoryloxy)methyl)-2,2-dimethyl-5-(pentadec-1''-enyl)oxazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydroxide / water / 20 °C

2.1: 1H-imidazole / dichloromethane / 3 h / 20 °C

2.2: 0.5 h / Reflux

2.3: 6 h / 20 °C

3.1: 1H-tetrazole / acetonitrile / 3 h / 20 °C

4.1: di-tert-butyl peroxide / toluene / 1 h / 20 °C

5.1: lithium iodide / pyridine / Reflux

With 1H-imidazole; 1H-tetrazole; di-tert-butyl peroxide; sodium hydroxide; lithium iodide; In pyridine; dichloromethane; water; toluene; acetonitrile;

Reference yield:

: 116467-63-1
N-tert-butyloxycarbonylsphingosine

: 1196664-91-1
tert-butyl (4S,5R,1''E)-4-((((4'-bromo-5'-hydroxy-2'-nitrophenyl)(phenyl)methoxy)(hydroxy)phosphoryloxy)methyl)-2,2-dimethyl-5-(pentadec-1''-enyl)oxazolidine-3-carboxylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole / dichloromethane / 3 h / 20 °C

1.2: 0.5 h / Reflux

1.3: 6 h / 20 °C

2.1: 1H-tetrazole / acetonitrile / 3 h / 20 °C

3.1: di-tert-butyl peroxide / toluene / 1 h / 20 °C

4.1: lithium iodide / pyridine / Reflux

With 1H-imidazole; 1H-tetrazole; di-tert-butyl peroxide; lithium iodide; In pyridine; dichloromethane; toluene; acetonitrile;