2-[(Z)-(3,5-dimethyl-2H-pyrrol-2-ylidene)(4-iodophenyl)methyl]-3,5-dimethyl-1H-pyrrole

Base Information

Chemical Name:2-[(Z)-(3,5-dimethyl-2H-pyrrol-2-ylidene)(4-iodophenyl)methyl]-3,5-dimethyl-1H-pyrrole
CAS No.:945587-99-5
Molecular Formula:C₁₉H₁₉IN₂
Molecular Weight:402.278
Hs Code.:

Synonyms:2-[(Z)-(3,5-dimethyl-2H-pyrrol-2-ylidene)(4-iodophenyl)methyl]-3,5-dimethyl-1H-pyrrole

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Chemical Property of 2-[(Z)-(3,5-dimethyl-2H-pyrrol-2-ylidene)(4-iodophenyl)methyl]-3,5-dimethyl-1H-pyrrole

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Technology Process of 2-[(Z)-(3,5-dimethyl-2H-pyrrol-2-ylidene)(4-iodophenyl)methyl]-3,5-dimethyl-1H-pyrrole

There total 4 articles about 2-[(Z)-(3,5-dimethyl-2H-pyrrol-2-ylidene)(4-iodophenyl)methyl]-3,5-dimethyl-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 945587-86-0
2-(4-iodobenzoyl)-3,5-dimethylpyrrole

: 945587-99-5
2-[(Z)-(3,5-dimethyl-2H-pyrrol-2-ylidene)(4-iodophenyl)methyl]-3,5-dimethyl-1H-pyrrole

Guidance literature:: With trichlorophosphate; In dichloromethane; pentane; at 20 ℃; for 24h;
DOI:10.1021/jo061567m

Reference yield: 24.0%

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 619-58-9
4-iodobenzoic acid

: 945587-99-5
2-[(Z)-(3,5-dimethyl-2H-pyrrol-2-ylidene)(4-iodophenyl)methyl]-3,5-dimethyl-1H-pyrrole

Guidance literature:: 4-iodobenzoic acid; With trichlorophosphate; for 1h; Heating;

2,4-dimethyl-1H-pyrrole; for 1h; Heating;
DOI:10.1021/jo061567m

Reference yield:

: 625-82-1
2,4-dimethyl-1H-pyrrole

: 945587-99-5
2-[(Z)-(3,5-dimethyl-2H-pyrrol-2-ylidene)(4-iodophenyl)methyl]-3,5-dimethyl-1H-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / CH₃MgBr / diethyl ether / 12 h / 20 °C

2: 46 percent / phosphorus oxychloride / pentane; CH₂Cl₂ / 24 h / 20 °C

With methylmagnesium bromide; trichlorophosphate; In diethyl ether; dichloromethane; pentane;
DOI:10.1021/jo061567m