4-fluoro-N-(3-fluoro-4-(5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)-2-methylbenzamide

Base Information

Chemical Name:4-fluoro-N-(3-fluoro-4-(5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)-2-methylbenzamide
CAS No.:1431386-67-2
Molecular Formula:C₁₉H₁₄F₅N₃O
Molecular Weight:395.332
Hs Code.:

Synonyms:4-fluoro-N-(3-fluoro-4-(5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)-2-methylbenzamide

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Chemical Property of 4-fluoro-N-(3-fluoro-4-(5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)-2-methylbenzamide

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Technology Process of 4-fluoro-N-(3-fluoro-4-(5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)-2-methylbenzamide

There total 4 articles about 4-fluoro-N-(3-fluoro-4-(5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)-2-methylbenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.5%

: 1006960-93-5
3-fluoro-4-(5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)aniline

: 21900-43-6
4-fluoro-2-methylbenzoyl chloride

: 1431386-67-2
4-fluoro-N-(3-fluoro-4-(5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)-2-methylbenzamide

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;

Reference yield:

: 369-34-6
3,4-difluoronitrobenzene

: 1431386-67-2
4-fluoro-N-(3-fluoro-4-(5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)-2-methylbenzamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / dimethyl sulfoxide / 0.5 h / 120 °C

1.2: 4 h / 120 °C

2.1: hydrogen; palladium on activated charcoal / methanol / 2 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With palladium on activated charcoal; hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; dimethyl sulfoxide;

Reference yield:

: 1431386-81-0
C₁₁H₇F₄N₃O₂

: 1431386-67-2
4-fluoro-N-(3-fluoro-4-(5-methyl-3-(trifluoromethyl)-1H-pyrazol-1-yl)phenyl)-2-methylbenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen; palladium on activated charcoal / methanol / 2 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With palladium on activated charcoal; hydrogen; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane;