C₁₁H₁₃BrClNO₃*ClH

Base Information

Chemical Name:C₁₁H₁₃BrClNO₃*ClH
CAS No.:1432502-43-6
Molecular Formula:C₁₁H₁₃BrClNO₃*ClH
Molecular Weight:359.047
Hs Code.:

C<sub>11</sub>H<sub>13</sub>BrClNO<sub>3</sub>*ClH

Synonyms:C₁₁H₁₃BrClNO₃*ClH

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Chemical Property of C₁₁H₁₃BrClNO₃*ClH

Chemical Property:

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Technology Process of C₁₁H₁₃BrClNO₃*ClH

There total 12 articles about C₁₁H₁₃BrClNO₃*ClH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1432502-42-5
C₁₆H₁₉BrClNO₃

: 1432502-43-6
C₁₁H₁₃BrClNO₃*ClH

Guidance literature:: With hydrogenchloride; water; Reflux;

Reference yield:

: 1432502-36-7
C₁₄H₁₇BrClNO₄

: 1432502-43-6
C₁₁H₁₃BrClNO₃*ClH

Guidance literature:: Multi-step reaction with 7 steps

1.1: dmap / dichloromethane / 0.17 h / -5 °C / Inert atmosphere

1.2: -5 - 20 °C

2.1: acetic acid / dichloromethane / 0.17 h / 0 °C

2.2: 1 h / 0 °C

3.1: toluene / 2 h / Reflux

4.1: trifluoroacetic acid / dichloromethane / 4 h / 0 °C

5.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C / Inert atmosphere

5.2: 2 h

6.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere

6.2: -78 °C

7.1: hydrogenchloride; water / Reflux

With hydrogenchloride; dmap; water; sodium hexamethyldisilazane; sodium hydride; acetic acid; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; toluene; mineral oil;

Reference yield:

: 1213929-66-8,444727-07-5
C₉H₉BrClNO₂

: 1432502-43-6
C₁₁H₁₃BrClNO₃*ClH

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydroxide / water; acetonitrile / 0 - 20 °C

2.1: dmap / dichloromethane / 0.17 h / -5 °C / Inert atmosphere

2.2: -5 - 20 °C

3.1: acetic acid / dichloromethane / 0.17 h / 0 °C

3.2: 1 h / 0 °C

4.1: toluene / 2 h / Reflux

5.1: trifluoroacetic acid / dichloromethane / 4 h / 0 °C

6.1: sodium hydride / tetrahydrofuran; mineral oil / 1 h / 0 °C / Inert atmosphere

6.2: 2 h

7.1: sodium hexamethyldisilazane / tetrahydrofuran / -78 °C / Inert atmosphere

7.2: -78 °C

8.1: hydrogenchloride; water / Reflux

With hydrogenchloride; dmap; water; sodium hexamethyldisilazane; sodium hydride; acetic acid; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile; mineral oil;