diphenyl 5-fluorothiazol-2-ylphosphoramidate

Base Information

Chemical Name:diphenyl 5-fluorothiazol-2-ylphosphoramidate
CAS No.:1334496-09-1
Molecular Formula:C₁₅H₁₂FN₂O₃PS
Molecular Weight:350.31
Hs Code.:

Synonyms:diphenyl 5-fluorothiazol-2-ylphosphoramidate

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Chemical Property of diphenyl 5-fluorothiazol-2-ylphosphoramidate

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Technology Process of diphenyl 5-fluorothiazol-2-ylphosphoramidate

There total 3 articles about diphenyl 5-fluorothiazol-2-ylphosphoramidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1334496-14-8
2-(diphenoxyphosphorylamino)thiazole-5-carboxylic acid

: 1334496-09-1
diphenyl 5-fluorothiazol-2-ylphosphoramidate

Guidance literature:: With 1-(chloromethyl)-4-fluoro-1,4-diazabicyclo[2.2.2]octane-1,4-diium tetrafluoroborate; In 2-methyltetrahydrofuran; water; at 2 - 20 ℃; for 4h;

Reference yield:

: 1334496-13-7
methyl 2-(diphenoxyphosphorylamino)thiazole-5-carboxylate

: 1334496-09-1
diphenyl 5-fluorothiazol-2-ylphosphoramidate

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide; water / methanol / 20 °C

1.2: 2 h / 20 °C / pH 2

2.1: 1-(chloromethyl)-4-fluoro-1,4-diazabicyclo[2.2.2]octane-1,4-diium tetrafluoroborate / water; 2-methyltetrahydrofuran / 4 h / 2 - 20 °C

With 1-(chloromethyl)-4-fluoro-1,4-diazabicyclo[2.2.2]octane-1,4-diium tetrafluoroborate; water; potassium hydroxide; In 2-methyltetrahydrofuran; methanol; water;

Reference yield:

: 2524-64-3
chlorophosphoric acid diphenyl ester

: 1334496-09-1
diphenyl 5-fluorothiazol-2-ylphosphoramidate

Guidance literature:: Multi-step reaction with 3 steps

1.1: 4-methyl-morpholine / 20 °C / Cooling with ice

2.1: potassium hydroxide; water / methanol / 20 °C

2.2: 2 h / 20 °C / pH 2

3.1: 1-(chloromethyl)-4-fluoro-1,4-diazabicyclo[2.2.2]octane-1,4-diium tetrafluoroborate / water; 2-methyltetrahydrofuran / 4 h / 2 - 20 °C

With 1-(chloromethyl)-4-fluoro-1,4-diazabicyclo[2.2.2]octane-1,4-diium tetrafluoroborate; water; potassium hydroxide; In 2-methyltetrahydrofuran; 4-methyl-morpholine; methanol; water;