1H-INDEN-1-AMINE, 5-BROMO-2,3-DIHYDRO-

Base Information

• Chemical Name: 1H-INDEN-1-AMINE, 5-BROMO-2,3-DIHYDRO-
• CAS No.: 185122-74-1
• Molecular Formula: C9H10 Br N
• Molecular Weight: 212.089
• Hs Code.: 2921499090
• Mol file: 185122-74-1.mol

Synonyms:(5-Bromoindan-1-yl)amine;5-Bromo-1-indanamine; 5-Bromo-2,3-dihydro-1H-inden-1-amine

Chemical Property of 1H-INDEN-1-AMINE, 5-BROMO-2,3-DIHYDRO-

Chemical Property:

• Boiling Point: 278.2±40.0 °C(Predicted)
• PKA: 9.05±0.20(Predicted)
• PSA: 26.02000
• Density: 1.490±0.06 g/cm3(Predicted)
• LogP: 3.09540
• Storage Temp.: 2-8°C(protect from light)

Purity/Quality:

99%, ^*data from raw suppliers

5-Bromo-indan-1-ylamine 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-INDEN-1-AMINE, 5-BROMO-2,3-DIHYDRO-

There total 10 articles about 1H-INDEN-1-AMINE, 5-BROMO-2,3-DIHYDRO- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

5-bromo-2,3-dihydro-1H-inden-1-one oxime (185122-63-8) → 5-bromo-2,3-dihydro-1H-inden-1-one oxime (185122-74-1)

Guidance literature:

5-bromo-2,3-dihydro-1H-inden-1-one oxime; With lithium aluminium tetrahydride; In diethyl ether; at -78 ℃; for 5h; Cooling with acetone-dry ice; Heating / reflux;

With sodium hydroxide; In diethyl ether; water; at 0 - 5 ℃;

Reference yield: 94.0%

5-bromo-indan-1-one oxime (1251457-83-6) → 5-bromo-2,3-dihydro-1H-inden-1-one oxime (185122-74-1)

Guidance literature:

5-bromo-indan-1-one oxime; With lithium aluminium tetrahydride; In diethyl ether; at -78 - 40 ℃; for 5h;

With sodium hydroxide; water; In diethyl ether; at 0 ℃; Product distribution / selectivity;

Reference yield: 85.0%

1-azido-5-bromo-2,3-dihydro-1H-indene (701268-37-3) → 5-bromo-2,3-dihydro-1H-inden-1-one oxime (185122-74-1)

Guidance literature:

1-azido-5-bromo-2,3-dihydro-1H-indene; With lithium aluminium tetrahydride; In tetrahydrofuran; at -15 - 20 ℃;

With water; In tetrahydrofuran; at -10 - 20 ℃; for 4h;

upstream raw materials:

1-azido-5-bromo-2,3-dihydro-1H-indene

5-bromo-indan-1-one oxime

5-bromo-2,3-dihydro-1H-inden-1-one oxime

5-Bromo-1-indanone

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