3-hydroxyumbilicaric acid

Base Information

Chemical Name:3-hydroxyumbilicaric acid
CAS No.:124281-21-6
Molecular Formula:C₂₅H₂₂O₁₁
Molecular Weight:498.443
Hs Code.:

Synonyms:3-hydroxyumbilicaric acid

Suppliers and Price of 3-hydroxyumbilicaric acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 3-hydroxyumbilicaric acid

Chemical Property:

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

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Technology Process of 3-hydroxyumbilicaric acid

There total 7 articles about 3-hydroxyumbilicaric acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 124281-20-5
benzyl 3-benzyloxy-4-O-benzylumbilicarate

: 124281-21-6
3-hydroxyumbilicaric acid

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; for 4h;

Reference yield:

: 61158-13-2
benzyl lecanorate

: 124281-21-6
3-hydroxyumbilicaric acid

Guidance literature:: Multi-step reaction with 2 steps

1: 44 percent / trifluoroacetic anhydride / toluene / 4 h / Ambient temperature

2: 18 percent / H₂ / 10percent Pd/C / ethyl acetate / 4 h

With hydrogen; trifluoroacetic anhydride; palladium on activated charcoal; In ethyl acetate; toluene;

Reference yield:

: 124281-12-5
ethyl 4-benzyloxy-3-formyl-2-hydroxy-6-methylbenzoate

: 124281-21-6
3-hydroxyumbilicaric acid

Guidance literature:: Multi-step reaction with 6 steps

1: 87 percent / K₂CO₃ / dimethylformamide / 24 h / Ambient temperature

2: 2.42 g / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / Ambient temperature

3: 77 percent / K₂CO₃ / acetone / 22 h / Heating

4: 85 percent / KOH / H₂O; dimethylsulfoxide / 3 h / 90 °C

5: 44 percent / trifluoroacetic anhydride / toluene / 4 h / Ambient temperature

6: 18 percent / H₂ / 10percent Pd/C / ethyl acetate / 4 h

With potassium hydroxide; hydrogen; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; palladium on activated charcoal; In dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide; acetone; toluene;