benzyl 3-benzyloxy-4-O-benzylumbilicarate

Base Information

Chemical Name:benzyl 3-benzyloxy-4-O-benzylumbilicarate
CAS No.:124281-20-5
Molecular Formula:C₄₆H₄₀O₁₁
Molecular Weight:768.817
Hs Code.:

Synonyms:benzyl 3-benzyloxy-4-O-benzylumbilicarate

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Chemical Property of benzyl 3-benzyloxy-4-O-benzylumbilicarate

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Technology Process of benzyl 3-benzyloxy-4-O-benzylumbilicarate

There total 5 articles about benzyl 3-benzyloxy-4-O-benzylumbilicarate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 124281-20-5
benzyl 3-benzyloxy-4-O-benzylumbilicarate

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / K₂CO₃ / acetone / 22 h / Heating

2: 85 percent / KOH / H₂O; dimethylsulfoxide / 3 h / 90 °C

3: 44 percent / trifluoroacetic anhydride / toluene / 4 h / Ambient temperature

With potassium hydroxide; potassium carbonate; trifluoroacetic anhydride; In water; dimethyl sulfoxide; acetone; toluene;

Reference yield:

: 124281-12-5
ethyl 4-benzyloxy-3-formyl-2-hydroxy-6-methylbenzoate

: 124281-20-5
benzyl 3-benzyloxy-4-O-benzylumbilicarate

Guidance literature:: Multi-step reaction with 5 steps

1: 87 percent / K₂CO₃ / dimethylformamide / 24 h / Ambient temperature

2: 2.42 g / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / Ambient temperature

3: 77 percent / K₂CO₃ / acetone / 22 h / Heating

4: 85 percent / KOH / H₂O; dimethylsulfoxide / 3 h / 90 °C

5: 44 percent / trifluoroacetic anhydride / toluene / 4 h / Ambient temperature

With potassium hydroxide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene;

Reference yield:

: 124281-15-8
ethyl 4-benzyloxy-3-formyl-2-methoxy-6-methylbenzoate

: 124281-20-5
benzyl 3-benzyloxy-4-O-benzylumbilicarate

Guidance literature:: Multi-step reaction with 4 steps

1: 2.42 g / m-chloroperbenzoic acid / CH₂Cl₂ / 1 h / Ambient temperature

2: 77 percent / K₂CO₃ / acetone / 22 h / Heating

3: 85 percent / KOH / H₂O; dimethylsulfoxide / 3 h / 90 °C

4: 44 percent / trifluoroacetic anhydride / toluene / 4 h / Ambient temperature

With potassium hydroxide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In dichloromethane; water; dimethyl sulfoxide; acetone; toluene;