tert-butyl (S)-3'-phenyl-2'-([1R,2E,4R]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylideneamino)propanoate

Base Information

Chemical Name:tert-butyl (S)-3'-phenyl-2'-([1R,2E,4R]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylideneamino)propanoate
CAS No.:334817-48-0
Molecular Formula:C₂₃H₃₃NO₂
Molecular Weight:355.521
Hs Code.:

Synonyms:tert-butyl (S)-3'-phenyl-2'-([1R,2E,4R]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylideneamino)propanoate

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Chemical Property of tert-butyl (S)-3'-phenyl-2'-([1R,2E,4R]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylideneamino)propanoate

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Technology Process of tert-butyl (S)-3'-phenyl-2'-([1R,2E,4R]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylideneamino)propanoate

There total 4 articles about tert-butyl (S)-3'-phenyl-2'-([1R,2E,4R]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylideneamino)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 287488-25-9
(1R,4R)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-imine

: 15100-75-1,75898-47-4
L-phenylalanine tert-butyl ester hydrochloride

: 334817-48-0
tert-butyl (S)-3'-phenyl-2'-([1R,2E,4R]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylideneamino)propanoate

Guidance literature:: In diethyl ether; dichloromethane; at 23 ℃;
DOI:10.1039/b007659g

Reference yield:

: 464-49-3,68546-28-1
(1R,4R)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one

: 334817-48-0
tert-butyl (S)-3'-phenyl-2'-([1R,2E,4R]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylideneamino)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / hydroxylamine hydrochloride; aq. sodium acetate / ethanol / 15 h / 60 °C

2: n-Bu₃P; PhSSPh / tetrahydrofuran / 2.5 h / 20 °C

3: 70 percent / diethyl ether; CH₂Cl₂ / 23 °C

With tributylphosphine; hydroxylamine hydrochloride; sodium acetate; diphenyldisulfane; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane;
DOI:10.1039/b007659g

Reference yield:

: 2792-42-9
(R,R)-camphor oxime

: 334817-48-0
tert-butyl (S)-3'-phenyl-2'-([1R,2E,4R]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylideneamino)propanoate

Guidance literature:: Multi-step reaction with 2 steps

1: n-Bu₃P; PhSSPh / tetrahydrofuran / 2.5 h / 20 °C

2: 70 percent / diethyl ether; CH₂Cl₂ / 23 °C

With tributylphosphine; diphenyldisulfane; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1039/b007659g