Bicyclo[2.2.1]heptan-2-imine, 1,7,7-trimethyl-, (1R,4R)- (9CI)

Base Information

• Chemical Name: Bicyclo[2.2.1]heptan-2-imine, 1,7,7-trimethyl-, (1R,4R)- (9CI)
• CAS No.: 287488-25-9
• Molecular Formula: C10H17 N
• Molecular Weight: 151.252
• Mol file: 287488-25-9.mol

Synonyms:Bicyclo[2.2.1]heptan-2-imine, 1,7,7-trimethyl-, (1R,4R)- (9CI)

Chemical Property of Bicyclo[2.2.1]heptan-2-imine, 1,7,7-trimethyl-, (1R,4R)- (9CI)

Chemical Property:

• PSA: 23.85000
• LogP: 2.95210

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Bicyclo[2.2.1]heptan-2-imine, 1,7,7-trimethyl-, (1R,4R)- (9CI)

There total 6 articles about Bicyclo[2.2.1]heptan-2-imine, 1,7,7-trimethyl-, (1R,4R)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (1R,4R)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-imine (287488-25-9) + benzaldehyde (100-52-7)

Guidance literature:

bei der Destillation;

Reference yield:

(1R,4R)-1-oxo-2-(1,7,7-trimethylbicyclo[2.2.1]hept-2-ylidene)-hydrazinium-1-olate (1191099-59-8) → (1R,4R)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-imine (287488-25-9)

Guidance literature:

With ammonia; In tetrahydrofuran; at 0 ℃; for 4h;

DOI:10.1021/jo000176j

Reference yield:

(R,R)-camphor oxime (2792-42-9) → (1R,4R)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-imine (287488-25-9)

Guidance literature:

Reaktion ueber mehrere Stufen;

upstream raw materials:

N-nitrocaphorimine

(R,R)-camphor oxime

(1R,4R)-1-oxo-2-(1,7,7-trimethylbicyclo[2.2.1]hept-2-ylidene)-hydrazinium-1-olate

(1R,4R)-1,7,7-trimethylbicyclo[2.2.1]heptan-2-one

Downstream raw materials:

Camphor

methyl (S)-3'-phenyl-2'-([1R,2E,4R]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylideneamino)propanoate

tert-butyl (S)-3'-phenyl-2'-([1R,2E,4R]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylideneamino)propanoate

tert-butyl (R)-3'-phenyl-2'-([1R,2E,4R]-1,7,7-trimethylbicyclo[2.2.1]heptan-2-ylideneamino)propanoate

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