2-azido-2-deoxy-4-O-p-methoxybenzyl-3-O-triisopropylsilyl-D-sorbitol

Base Information

Chemical Name:2-azido-2-deoxy-4-O-p-methoxybenzyl-3-O-triisopropylsilyl-D-sorbitol
CAS No.:1338594-63-0
Molecular Formula:C₂₃H₄₁N₃O₆Si
Molecular Weight:483.681
Hs Code.:

Synonyms:2-azido-2-deoxy-4-O-p-methoxybenzyl-3-O-triisopropylsilyl-D-sorbitol

Suppliers and Price of 2-azido-2-deoxy-4-O-p-methoxybenzyl-3-O-triisopropylsilyl-D-sorbitol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-azido-2-deoxy-4-O-p-methoxybenzyl-3-O-triisopropylsilyl-D-sorbitol

Chemical Property:

Purity/Quality:

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Technology Process of 2-azido-2-deoxy-4-O-p-methoxybenzyl-3-O-triisopropylsilyl-D-sorbitol

There total 6 articles about 2-azido-2-deoxy-4-O-p-methoxybenzyl-3-O-triisopropylsilyl-D-sorbitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₃₉N₃O₆Si

: 1338594-63-0
2-azido-2-deoxy-4-O-p-methoxybenzyl-3-O-triisopropylsilyl-D-sorbitol

Guidance literature:: With sodium tetrahydroborate; water; In ethanol; Product distribution / selectivity;

Reference yield:

: 2-azido-2-deoxy-D-glucose

: 1338594-63-0
2-azido-2-deoxy-4-O-p-methoxybenzyl-3-O-triisopropylsilyl-D-sorbitol

Guidance literature:: Multi-step reaction with 8 steps

1: pyridine

2: boron trifluoride diethyl etherate / dichloromethane

3: sodium methylate; methanol

4: camphor-10-sulfonic acid / acetonitrile

5: N-ethyl-N,N-diisopropylamine / dichloromethane

6: di-n-butylboryl trifluoromethanesulfonate; borane / tetrahydrofuran / 0 °C

7: N-Bromosuccinimide; water / acetone

8: water; sodium tetrahydroborate / ethanol

With pyridine; methanol; sodium tetrahydroborate; N-Bromosuccinimide; di-n-butylboryl trifluoromethanesulfonate; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; borane; water; sodium methylate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; acetone; acetonitrile;

Reference yield:

: 171032-74-9
1,3,4,6-tetra-O-acetyl-2-azido-2-deoxy-D-glucopyranose

: 1338594-63-0
2-azido-2-deoxy-4-O-p-methoxybenzyl-3-O-triisopropylsilyl-D-sorbitol

Guidance literature:: Multi-step reaction with 7 steps

1: boron trifluoride diethyl etherate / dichloromethane

2: sodium methylate; methanol

3: camphor-10-sulfonic acid / acetonitrile

4: N-ethyl-N,N-diisopropylamine / dichloromethane

5: di-n-butylboryl trifluoromethanesulfonate; borane / tetrahydrofuran / 0 °C

6: N-Bromosuccinimide; water / acetone

7: water; sodium tetrahydroborate / ethanol

With methanol; sodium tetrahydroborate; N-Bromosuccinimide; di-n-butylboryl trifluoromethanesulfonate; camphor-10-sulfonic acid; boron trifluoride diethyl etherate; borane; water; sodium methylate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethanol; dichloromethane; acetone; acetonitrile;