13-cyclohexyl-3-methoxy-6-[2-(methoxycarbonyl)-3-thienyl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 1,1-dimethylethyl ester

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Chemical Name:13-cyclohexyl-3-methoxy-6-[2-(methoxycarbonyl)-3-thienyl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 1,1-dimethylethyl ester
CAS No.:1127234-57-4
Molecular Formula:C₃₅H₃₇NO₅S
Molecular Weight:583.748
Hs Code.:

Synonyms:13-cyclohexyl-3-methoxy-6-[2-(methoxycarbonyl)-3-thienyl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 1,1-dimethylethyl ester

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Chemical Property of 13-cyclohexyl-3-methoxy-6-[2-(methoxycarbonyl)-3-thienyl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 1,1-dimethylethyl ester

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Technology Process of 13-cyclohexyl-3-methoxy-6-[2-(methoxycarbonyl)-3-thienyl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 1,1-dimethylethyl ester

There total 1 articles about 13-cyclohexyl-3-methoxy-6-[2-(methoxycarbonyl)-3-thienyl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 26137-08-6
methyl 3-bromothiophene-2-carboxylate

: 945627-36-1
7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid, 13-cyclohexyl-3-methoxy-6-(tributylstannyl)-, 1,1-dimethylethyl ester

: 1127234-57-4
13-cyclohexyl-3-methoxy-6-[2-(methoxycarbonyl)-3-thienyl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 1,1-dimethylethyl ester

Guidance literature:: bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; at 100 ℃; for 4.5h;

Reference yield:

: 1127234-57-4
13-cyclohexyl-3-methoxy-6-[2-(methoxycarbonyl)-3-thienyl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 1,1-dimethylethyl ester

: 1127234-58-5
6-(2-carboxy-3-thienyl)-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 10-(1,1-dimethylethyl)ester

Guidance literature:: 13-cyclohexyl-3-methoxy-6-[2-(methoxycarbonyl)-3-thienyl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 1,1-dimethylethyl ester; With tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 24h;

With citric acid; In tetrahydrofuran; methanol; dichloromethane;