6-(2-carboxy-3-thienyl)-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 10-(1,1-dimethylethyl)ester

Base Information

Chemical Name:6-(2-carboxy-3-thienyl)-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 10-(1,1-dimethylethyl)ester
CAS No.:1127234-58-5
Molecular Formula:C₃₄H₃₅NO₅S
Molecular Weight:569.722
Hs Code.:

Synonyms:6-(2-carboxy-3-thienyl)-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 10-(1,1-dimethylethyl)ester

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Chemical Property of 6-(2-carboxy-3-thienyl)-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 10-(1,1-dimethylethyl)ester

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Technology Process of 6-(2-carboxy-3-thienyl)-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 10-(1,1-dimethylethyl)ester

There total 1 articles about 6-(2-carboxy-3-thienyl)-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 10-(1,1-dimethylethyl)ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1127234-57-4
13-cyclohexyl-3-methoxy-6-[2-(methoxycarbonyl)-3-thienyl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 1,1-dimethylethyl ester

: 1127234-58-5
6-(2-carboxy-3-thienyl)-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 10-(1,1-dimethylethyl)ester

Guidance literature:: 13-cyclohexyl-3-methoxy-6-[2-(methoxycarbonyl)-3-thienyl]-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 1,1-dimethylethyl ester; With tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 24h;

With citric acid; In tetrahydrofuran; methanol; dichloromethane;

Reference yield:

: 1127234-58-5
6-(2-carboxy-3-thienyl)-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 10-(1,1-dimethylethyl)ester

: 109-89-7
diethylamine

: 1127234-59-6
13-cyclohexyl-6-[2-[(diethylamino)carbonyl]-3-thienyl]-3-methoxy-7H-indolo[2,1-a] [2]benzazepine-10-carboxylic acid 1,1-dimethylethyl ester

Guidance literature:: 6-(2-carboxy-3-thienyl)-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 10-(1,1-dimethylethyl)ester; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In N,N-dimethyl-formamide; at 20 ℃; for 1.5h;

diethylamine; With dmap; In N,N-dimethyl-formamide; at 20 ℃; for 21h;

Reference yield:

: 110-91-8,99108-56-2
morpholine

: 1127234-58-5
6-(2-carboxy-3-thienyl)-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 10-(1,1-dimethylethyl)ester

: 1127234-64-3
tert-butyl 13-cyclohexyl-3-methoxy-6-(2-(morpholin-4-ylcarbonyl)-3-thienyl)-7H-indolo[2,1-a][2]benzazepine-10-carboxylate

Guidance literature:: 6-(2-carboxy-3-thienyl)-13-cyclohexyl-3-methoxy-7H-indolo[2,1-a][2]benzazepine-10-carboxylic acid 10-(1,1-dimethylethyl)ester; With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; In N,N-dimethyl-formamide; at 20 ℃; for 1.33333h;

morpholine; With dmap; In N,N-dimethyl-formamide; at 20 ℃; for 48h;