allyl 2-O-acetyl-3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranoside

Base Information

Chemical Name:allyl 2-O-acetyl-3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranoside
CAS No.:1240486-85-4
Molecular Formula:C₂₅H₄₀O₇Si
Molecular Weight:480.674
Hs Code.:

Synonyms:allyl 2-O-acetyl-3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 2-O-acetyl-3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranoside

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Technology Process of allyl 2-O-acetyl-3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranoside

There total 1 articles about allyl 2-O-acetyl-3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1240486-82-1
allyl 2-O-acetyl-3-O-p-methoxybenzyl-α-L-rhamnopyranoside

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1240486-85-4
allyl 2-O-acetyl-3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranoside

Guidance literature:: With 1H-imidazole; dmap; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo101231r

Reference yield:

: 1240486-85-4
allyl 2-O-acetyl-3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranoside

: C₂₂H₃₆O₇Si

Guidance literature:: With sodium acetate; palladium dichloride; In water; acetic acid; at 30 ℃;
DOI:10.1021/ol4020255

Reference yield:

: 1240486-85-4
allyl 2-O-acetyl-3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranoside

: 1448686-56-3
2-O-acetyl-3-O-p-methoxybenzyl-4-O-tert-butyldimethylsilyl-α-L-rhamnopyranosyl trichloroacetimidate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium dichloride; sodium acetate / acetic acid; water / 30 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 5 h / 0 °C

With sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium dichloride; In dichloromethane; water; acetic acid;
DOI:10.1021/ol4020255