Technology Process of C29H28N2O
There total 5 articles about C29H28N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
samarium diiodide;
In
tetrahydrofuran; methanol;
at 20 ℃;
for 0.166667h;
DOI:10.1021/ja405444c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (R)-3,3'-bis(dimethylphenylsilyl)-1,1'-binaphthyl-2,2'-dicarboxylic acid; 2,6-bis[(4R)-5,5-dihydro-4-phenyl-2-oxazolyl]pyridine; copper diacetate / dichloromethane / 72 h / 40 °C / Inert atmosphere; Molecular sieve
2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 24 h / 20 °C
3: samarium diiodide / methanol; tetrahydrofuran / 0.17 h / 20 °C
With
samarium diiodide; palladium 10% on activated carbon; (R)-3,3'-bis(dimethylphenylsilyl)-1,1'-binaphthyl-2,2'-dicarboxylic acid; hydrogen; copper diacetate; 2,6-bis[(4R)-5,5-dihydro-4-phenyl-2-oxazolyl]pyridine;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja405444c
- Guidance literature:
-
Multi-step reaction with 3 steps
1: (R)-3,3'-bis(dimethylphenylsilyl)-1,1'-binaphthyl-2,2'-dicarboxylic acid; 2,6-bis[(4R)-5,5-dihydro-4-phenyl-2-oxazolyl]pyridine; copper diacetate / dichloromethane / 72 h / 40 °C / Inert atmosphere; Molecular sieve
2: palladium 10% on activated carbon; hydrogen / ethyl acetate / 24 h / 20 °C
3: samarium diiodide / methanol; tetrahydrofuran / 0.17 h / 20 °C
With
samarium diiodide; palladium 10% on activated carbon; (R)-3,3'-bis(dimethylphenylsilyl)-1,1'-binaphthyl-2,2'-dicarboxylic acid; hydrogen; copper diacetate; 2,6-bis[(4R)-5,5-dihydro-4-phenyl-2-oxazolyl]pyridine;
In
tetrahydrofuran; methanol; dichloromethane; ethyl acetate;
DOI:10.1021/ja405444c
