N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine isopentylamide

Base Information

Chemical Name:N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine isopentylamide
CAS No.:96866-05-6
Molecular Formula:C₁₈H₂₇N₃O₄
Molecular Weight:349.43
Hs Code.:

Synonyms:N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine isopentylamide

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Chemical Property of N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine isopentylamide

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Technology Process of N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine isopentylamide

There total 6 articles about N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine isopentylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 96866-18-1
N-<3(RS)--1-oxo-2-benzylpropyl>glycine isopentylamide

: 96866-05-6
N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine isopentylamide

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; for 3h; Ambient temperature;
DOI:10.1021/jm00147a007

Reference yield:

: 107-85-7
1-amino-3-methylbutane

: 96866-05-6
N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine isopentylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), DCC / tetrahydrofuran; CHCl₃ / Ambient temperature

2: 80 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), N-cyclohexyl-N'-<2-(4-morpholinyl)ethyl>carbodiimide methol p-toluenosulfonate / tetrahydrofuran / Ambient temperature

3: 70 percent / H₂ / 10percent Pd on charcoal / methanol / 3 h / Ambient temperature

With hydrogen; N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide; palladium on activated charcoal; In tetrahydrofuran; methanol; chloroform;
DOI:10.1021/jm00147a007

Reference yield:

: 5669-19-2
2-Benzyl-2-propenoic acid

: 96866-05-6
N-[3(RS)-(N-formyl-N-hydroxyamino)-1-oxo-2-benzylpropyl]glycine isopentylamide

Guidance literature:: Multi-step reaction with 4 steps

1: 57 percent / ethanol / 168 h / Heating

2: 98 percent / acetic anhydride / 3 h / 0 °C

3: 80 percent / Et₃N, 1-hydroxybenzotriazol (HOBT), N-cyclohexyl-N'-<2-(4-morpholinyl)ethyl>carbodiimide methol p-toluenosulfonate / tetrahydrofuran / Ambient temperature

4: 70 percent / H₂ / 10percent Pd on charcoal / methanol / 3 h / Ambient temperature

With hydrogen; acetic anhydride; N-cyclohexyl-N'-β-(4-methylmorpholinium)ethylcarbodiimide p-toluenesulfonate; benzotriazol-1-ol; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; ethanol;
DOI:10.1021/jm00147a007