4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine

Base Information

Chemical Name:4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine
CAS No.:1332527-86-2
Molecular Formula:C₂₄H₃₀N₄O₅S₂
Molecular Weight:518.658
Hs Code.:

Synonyms:4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine

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Chemical Property of 4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine

Chemical Property:

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Technology Process of 4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine

There total 9 articles about 4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1332527-56-6
4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine-1-carboxylic acid tert-butyl ester

: 1332527-86-2
4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 0.333333h;

Reference yield:

: 1332527-92-0
C₁₇H₂₅ClN₂O₆S₂

: 1332527-86-2
4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 3 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 0.33 h / 20 °C

With triethylamine; trifluoroacetic acid; In dichloromethane;

Reference yield:

: 6911-88-2
(2-bromo-4-nitro-phenyl)-methyl-amine

: 1332527-86-2
4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine

Guidance literature:: Multi-step reaction with 5 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / N,N-dimethyl-formamide / 23 h / 80 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C

3: palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

4: triethylamine / dichloromethane / 3 h / 20 °C

5: trifluoroacetic acid / dichloromethane / 0.33 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium on activated charcoal; hydrogen; sodium hydride; potassium carbonate; triethylamine; trifluoroacetic acid; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;