4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine-1-carboxylic acid tert-butyl ester

Base Information

Chemical Name:4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine-1-carboxylic acid tert-butyl ester
CAS No.:1332527-56-6
Molecular Formula:C₂₉H₃₈N₄O₇S₂
Molecular Weight:618.775
Hs Code.:

Synonyms:4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine-1-carboxylic acid tert-butyl ester

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Chemical Property of 4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine-1-carboxylic acid tert-butyl ester

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Technology Process of 4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine-1-carboxylic acid tert-butyl ester

There total 7 articles about 4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine-1-carboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1332527-92-0
C₁₇H₂₅ClN₂O₆S₂

: 158722-73-7
C₁₂H₁₄N₂O

: 1332527-56-6
4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine-1-carboxylic acid tert-butyl ester

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 1332527-89-5
C₁₁H₁₀N₂O₃

: 1332527-56-6
4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C

2: palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

3: triethylamine / dichloromethane / 3 h / 20 °C

With palladium on activated charcoal; hydrogen; sodium hydride; triethylamine; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 6911-88-2
(2-bromo-4-nitro-phenyl)-methyl-amine

: 1332527-56-6
4-{[3-(4-dimethylamino-3-furan-2-ylphenylsulfamoyl)benzenesulfonylamino]methyl}piperidine-1-carboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / N,N-dimethyl-formamide / 23 h / 80 °C / Inert atmosphere

2: sodium hydride / N,N-dimethyl-formamide / 3 h / 20 °C

3: palladium on activated charcoal; hydrogen / ethyl acetate / 20 °C

4: triethylamine / dichloromethane / 3 h / 20 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium on activated charcoal; hydrogen; sodium hydride; potassium carbonate; triethylamine; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide;